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[Ir(4-[2,2']bipyridinyl-5-ylethynylphenyl)bispyridin-2-ylmethylamine)(2-phenylpyridine)2]PF6

Base Information
  • Chemical Name:[Ir(4-[2,2']bipyridinyl-5-ylethynylphenyl)bispyridin-2-ylmethylamine)(2-phenylpyridine)2]PF6
  • CAS No.:1190325-69-9
  • Molecular Formula:C52H39IrN7*F6P
  • Molecular Weight:1099.11
  • Hs Code.:
[Ir(4-[2,2']bipyridinyl-5-ylethynylphenyl)bispyridin-2-ylmethylamine)(2-phenylpyridine)2]PF<sub>6</sub>

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Chemical Property of [Ir(4-[2,2']bipyridinyl-5-ylethynylphenyl)bispyridin-2-ylmethylamine)(2-phenylpyridine)2]PF6
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Technology Process of [Ir(4-[2,2']bipyridinyl-5-ylethynylphenyl)bispyridin-2-ylmethylamine)(2-phenylpyridine)2]PF6

There total 1 articles about [Ir(4-[2,2']bipyridinyl-5-ylethynylphenyl)bispyridin-2-ylmethylamine)(2-phenylpyridine)2]PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In methanol; dichloromethane; (Ar); using Schlenk techniques; reflux of mixt. of Ir2(C5H4NC6H4)4Cl2 and C5H4NC5H3NCCC6H4N(CH2C5H4N)2 in MeOH-CH2Cl2 (v/v = 1:2) with exclusionof light for 4 h; cooling to ambient temp.; addn. of soln. of KPF6 in M eOH; stirring for 30 min; evapn. to dryness; dissolving in CH2Cl2; chromy. on silica gel column using CH2Cl2-MeOH (v/v = 2:1) as eluent; elem. anal.;
DOI:10.1021/om900334f
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