bis of (-)-(S,S)-trans-10,11-dihydro-10,11-dihydroxy-5H-dibenzoazepine-5-carboxamide

Base Information

• Chemical Name: bis of (-)-(S,S)-trans-10,11-dihydro-10,11-dihydroxy-5H-dibenzoazepine-5-carboxamide
• CAS No.: 106680-76-6
• Molecular Formula: C₃₃H₃₂N₄O₅
• Molecular Weight: 564.641
• Mol file: 106680-76-6.mol

Synonyms:

Chemical Property of bis of (-)-(S,S)-trans-10,11-dihydro-10,11-dihydroxy-5H-dibenzoazepine-5-carboxamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis of (-)-(S,S)-trans-10,11-dihydro-10,11-dihydroxy-5H-dibenzoazepine-5-carboxamide

There total 1 articles about bis of (-)-(S,S)-trans-10,11-dihydro-10,11-dihydroxy-5H-dibenzoazepine-5-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(dimethylamino)benzoyl chloride (4755-50-4) + trans-10,11-Dihydroxycarbamazepine (106758-94-5,58955-93-4) → bis of (-)-(S,S)-trans-10,11-dihydro-10,11-dihydroxy-5H-dibenzoazepine-5-carboxamide (106680-76-6)

Guidance literature:

With pyridine; dmap; at 70 ℃; for 18h;

DOI:10.1021/jm00388a004

upstream raw materials:

4-(dimethylamino)benzoyl chloride

trans-10,11-Dihydroxycarbamazepine