((2-(i)Pr₂P-4-MeC₆H₃)2N)BF₂

Base Information

Chemical Name:((2-(i)Pr₂P-4-MeC₆H₃)2N)BF₂
CAS No.:1345840-97-2
Molecular Formula:C₂₆H₄₀BF₂NP₂
Molecular Weight:477.366
Hs Code.:

((2-(i)Pr<sub>2</sub>P-4-MeC<sub>6</sub>H<sub>3</sub>)2N)BF<sub>2</sub>

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Chemical Property of ((2-(i)Pr₂P-4-MeC₆H₃)2N)BF₂

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Technology Process of ((2-(i)Pr₂P-4-MeC₆H₃)2N)BF₂

There total 1 articles about ((2-(i)Pr₂P-4-MeC₆H₃)2N)BF₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 353-43-5
boron dimethyl-trifluoro sulphide

: 666856-94-6
2,2’-bis(diisopropylphosphino)-4,4’-ditolylamido

: 1345840-97-2
((2-(i)Pr₂P-4-MeC₆H₃)2N)BF₂

Guidance literature:: With n-C₄H₉Li; In hexane; toluene; (Ar); a soln. of n-C4H9Li in hexane added to a soln. of ligand in toluene, stirred for 10 min, protected from light and B complex added, stirredovernight; evapd. (vac.), filtered through a pad of Celite using Et2O, layered withpentane, cooled to -35°C while protected from light, sepd., wash ed (pentane), dried; elem. anal.;
DOI:10.1039/c1dt11172h