23-O-butyrylsilybin

Base Information

Chemical Name:23-O-butyrylsilybin
CAS No.:1220982-32-0
Molecular Formula:C₂₉H₂₈O₁₁
Molecular Weight:552.535
Hs Code.:

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Suppliers and Price of 23-O-butyrylsilybin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 23-O-butyrylsilybin

Chemical Property:

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Technology Process of 23-O-butyrylsilybin

There total 2 articles about 23-O-butyrylsilybin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 802918-57-6
silybin

: 141-75-3
butyryl chloride

: 1220982-32-0
23-O-butyrylsilybin

Guidance literature:: With boron trifluoride diethyl etherate; In diethyl ether; dichloromethane; acetonitrile; at 0 - 20 ℃; for 3h;
DOI:10.1021/np900758d

Reference yield: 28.0%

: silibinin

: 141-75-3
butyryl chloride

: 1220982-32-0
2-[2,3-dihydro-2-(butanoyloxymethyl)-3-(4-hydroxy-3-methoxyphenyl)-1,4-benzodioxin-6-yl]-2,3-dihydro-3,5,7-trihydroxy-4H-1-benzopyran-4-one

Guidance literature:: silibinin; butyryl chloride; With boron trifluoride diethyl etherate; In diethyl ether; dichloromethane; acetonitrile; at 0 - 20 ℃; for 3h;

With sodium hydrogencarbonate; In diethyl ether; dichloromethane; water; acetonitrile; for 0.166667h; Cooling with ice;
DOI:10.1016/j.ejmech.2009.11.056