chlorido(η6-p-cymene)(nalidixicato-κ2O,O')ruthenium(II)*toluene

Base Information

• Chemical Name: chlorido(η6-p-cymene)(nalidixicato-κ2O,O')ruthenium(II)*toluene
• CAS No.: 1290113-95-9
• Molecular Formula: C₇H₈*C₂₂H₂₅ClN₂O₃Ru
• Molecular Weight: 594.116
• Mol file: 1290113-95-9.mol

Synonyms:

Chemical Property of chlorido(η6-p-cymene)(nalidixicato-κ2O,O')ruthenium(II)*toluene

Chemical Property:

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Technology Process of chlorido(η6-p-cymene)(nalidixicato-κ2O,O')ruthenium(II)*toluene

There total 1 articles about chlorido(η6-p-cymene)(nalidixicato-κ2O,O')ruthenium(II)*toluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 (52462-29-0) + sodium nalidixicate hydrate + toluene (108-88-3,15644-74-3,16713-13-6) → chlorido(η6-p-cymene)(nalidixicato-κ2O,O')ruthenium(II)*toluene (1290113-95-9)

Guidance literature:

In methanol; chloroform; byproducts: NaCl; refluxing soln. of ruthenium compd. and sodium nalidixicate in CHCl3/methanol (1/1) for 6 h; filtration through celite, addn. of toluene, keeping at room temp. with slow evapn. for 3 d, isolation of crystals, washing with hexane, elem. anal.;

DOI:10.1021/om101180c

upstream raw materials:

[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

toluene