C₃₇H₅₅N₅O₈

Base Information

Chemical Name:C₃₇H₅₅N₅O₈
CAS No.:1333145-70-2
Molecular Formula:C₃₇H₅₅N₅O₈
Molecular Weight:697.872
Hs Code.:

C<sub>37</sub>H<sub>55</sub>N<sub>5</sub>O<sub>8</sub>

Synonyms:

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Chemical Property of C₃₇H₅₅N₅O₈

Chemical Property:

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Technology Process of C₃₇H₅₅N₅O₈

There total 21 articles about C₃₇H₅₅N₅O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2S,4R)-methyl 4-amino-2-methyl-5-phenylpentanoate hydrochloride

: 1333145-70-2
C₃₇H₅₅N₅O₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1-hydroxy-7-aza-benzotriazole; O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate

1.2: 0 - 20 °C

2.1: tetrahydrofuran; dichloromethane / 0 - 20 °C

3.1: 1-hydroxy-7-aza-benzotriazole; O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate

3.2: 0 - 20 °C

4.1: water; lithium hydroxide / tetrahydrofuran / 0 - 20 °C

5.1: pyridine

With pyridine; 1-hydroxy-7-aza-benzotriazole; O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; water; lithium hydroxide; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-0030-1260806

Reference yield:

: (2S,4R)-4-amino-2-methyl-5-phenylpentanoic acid hydrochloride

: 1333145-70-2
C₃₇H₅₅N₅O₈

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride; 2,2-dimethoxy-propane / Reflux

2.1: 1-hydroxy-7-aza-benzotriazole; O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate

2.2: 0 - 20 °C

3.1: tetrahydrofuran; dichloromethane / 0 - 20 °C

4.1: 1-hydroxy-7-aza-benzotriazole; O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate

4.2: 0 - 20 °C

5.1: water; lithium hydroxide / tetrahydrofuran / 0 - 20 °C

6.1: pyridine

With pyridine; hydrogenchloride; 1-hydroxy-7-aza-benzotriazole; O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; water; 2,2-dimethoxy-propane; lithium hydroxide; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-0030-1260806

Reference yield:

: 1333145-74-6
C₈H₁₁NO₄

: 1333145-70-2
C₃₇H₅₅N₅O₈

Guidance literature:: Multi-step reaction with 11 steps

1.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran

3.1: dimethylsulfide borane complex; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran / 0 °C

4.1: dichloromethane / 0 - 20 °C

5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride

5.2: 0 - 20 °C

6.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 0 - 20 °C

7.1: 1-hydroxy-7-aza-benzotriazole; O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate

7.2: 0 - 20 °C

8.1: tetrahydrofuran; dichloromethane / 0 - 20 °C

9.1: 1-hydroxy-7-aza-benzotriazole; O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate

9.2: 0 - 20 °C

10.1: water; lithium hydroxide / tetrahydrofuran / 0 - 20 °C

11.1: pyridine

With pyridine; 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; dimethylsulfide borane complex; water; sodium hydride; benzotriazol-1-ol; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; dichloromethane; 1.1: Dess-Martin oxidation;
DOI:10.1055/s-0030-1260806