C₄₉H₈₀O₉Si₂

Base Information

Chemical Name:C₄₉H₈₀O₉Si₂
CAS No.:954106-29-7
Molecular Formula:C₄₉H₈₀O₉Si₂
Molecular Weight:869.34
Hs Code.:

C<sub>49</sub>H<sub>80</sub>O<sub>9</sub>Si<sub>2</sub>

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Chemical Property of C₄₉H₈₀O₉Si₂

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Technology Process of C₄₉H₈₀O₉Si₂

There total 19 articles about C₄₉H₈₀O₉Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 954106-28-6
C₄₉H₈₄O₉Si₂

: 954106-29-7
C₄₉H₈₀O₉Si₂

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - 0 ℃; for 1.66667h;
DOI:10.1016/j.tetlet.2007.07.182

Reference yield:

: 954106-23-1
C₃₇H₄₅NO₆

: 954106-29-7
C₄₉H₈₀O₉Si₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: 92 percent / LiOH*H₂O; aq. H₂O₂ / tetrahydrofuran / 2 h / 20 °C

2.1: 96 percent / H₂; K₂CO₃ / Pd/C / methanol / 0.83 h

3.1: EDC; DMAP / dimethylformamide / 12 h / 50 °C

4.1: ((S)-1-Ph-2-piperidin-1-yl-Et)-(2,2,2-triF-Et)amine; n-BuLi / tetrahydrofuran; hexane / 1 h

4.2: Me₃SiCl / 0.58 h / -78 - 0 °C

5.1: 0.310 g / LiAlH₄ / tetrahydrofuran / 5 h / Heating

6.1: n-Bu₂SnO / toluene / 0.75 h / Heating

6.2: 71 percent / CH₂Cl₂ / 1 h / 0 °C

7.1: imidazole / dimethylformamide / 3 h / 65 °C

7.2: dimethylformamide / 20 h / 80 °C

8.1: 0.174 g / DDQ / CH₂Cl₂; H₂O / 1.5 h / 20 °C

9.1: O₃; N-methylmorpholine N-oxide; benzyl ethyl eter / CH₂Cl₂ / 0.13 h / -78 °C

9.2: 80 percent / NaBH₄ / methanol / 1 h / -40 - -10 °C

10.1: DMSO; (COCl)2; Et₃N / CH₂Cl₂ / 1.67 h / -78 - 0 °C

With 1H-imidazole; dmap; lithium hydroxide; lithium aluminium tetrahydride; n-butyllithium; oxalyl dichloride; hydrogen; dihydrogen peroxide; di(n-butyl)tin oxide; potassium carbonate; ozone; dimethyl sulfoxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; 4-methylmorpholine N-oxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; 4.1: Ireland-Claisen rearrngement / 10.1: Swern oxidation reaction;
DOI:10.1016/j.tetlet.2007.07.182

Reference yield:

: 954106-39-9
C₂₅H₃₁NO₄

: 954106-29-7
C₄₉H₈₀O₉Si₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: NaHDMS / tetrahydrofuran / 2 h / -78 °C

1.2: 80 percent / tetrahydrofuran / -78 - -20 °C

2.1: 92 percent / LiOH*H₂O; aq. H₂O₂ / tetrahydrofuran / 2 h / 20 °C

3.1: 96 percent / H₂; K₂CO₃ / Pd/C / methanol / 0.83 h

4.1: EDC; DMAP / dimethylformamide / 12 h / 50 °C

5.1: ((S)-1-Ph-2-piperidin-1-yl-Et)-(2,2,2-triF-Et)amine; n-BuLi / tetrahydrofuran; hexane / 1 h

5.2: Me₃SiCl / 0.58 h / -78 - 0 °C

6.1: 0.310 g / LiAlH₄ / tetrahydrofuran / 5 h / Heating

7.1: n-Bu₂SnO / toluene / 0.75 h / Heating

7.2: 71 percent / CH₂Cl₂ / 1 h / 0 °C

8.1: imidazole / dimethylformamide / 3 h / 65 °C

8.2: dimethylformamide / 20 h / 80 °C

9.1: 0.174 g / DDQ / CH₂Cl₂; H₂O / 1.5 h / 20 °C

10.1: O₃; N-methylmorpholine N-oxide; benzyl ethyl eter / CH₂Cl₂ / 0.13 h / -78 °C

10.2: 80 percent / NaBH₄ / methanol / 1 h / -40 - -10 °C

11.1: DMSO; (COCl)2; Et₃N / CH₂Cl₂ / 1.67 h / -78 - 0 °C

With 1H-imidazole; dmap; lithium hydroxide; lithium aluminium tetrahydride; n-butyllithium; oxalyl dichloride; hydrogen; dihydrogen peroxide; sodium hexamethyldisilazane; di(n-butyl)tin oxide; potassium carbonate; ozone; dimethyl sulfoxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; 4-methylmorpholine N-oxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; 5.1: Ireland-Claisen rearrngement / 11.1: Swern oxidation reaction;
DOI:10.1016/j.tetlet.2007.07.182