1-Tosylcyclam

Base Information

Chemical Name:1-Tosylcyclam
CAS No.:128495-29-4
Molecular Formula:C17H30N4O2S
Molecular Weight:354.517
Hs Code.:
UNII:787UTL3UF6
Nikkaji Number:J3.607.719K

Synonyms:1-Tosylcyclam;787UTL3UF6;1-Tosyl-1,4,8,11-Tetraazacyclotetradecane;1,4,8,11-Tetraazacyclotetradecane, 1-[(4-methylphenyl)sulfonyl]-;1-[(4-Methylphenyl)sulfonyl]-1,4,8,11-tetraazacyclotetradecane;128495-29-4

Suppliers and Price of 1-Tosylcyclam

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of 1-Tosylcyclam

Chemical Property:

XLogP3:0.6
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:354.20894739
Heavy Atom Count:24
Complexity:430

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)N2CCCNCCNCCCNCC2

Technology Process of 1-Tosylcyclam

There total 6 articles about 1-Tosylcyclam which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1-(p-toluenesulfonyl)-4,8,11-tris(trifluoroacetyl)-cyclam

: 128495-29-4
1-(4-tolylsulfonyl)-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: With potassium hydroxide; In methanol; for 1.5h; Heating;
DOI:10.1039/b311520h

Reference yield:

: 295-37-4
1,4,8,11-Tetraazacyclotetradecane

: 98-59-9
p-toluenesulfonyl chloride

: 128495-29-4
1-(4-tolylsulfonyl)-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: With triethylamine; In acetonitrile; at 70 ℃; for 12h;

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 128495-29-4
1-(4-tolylsulfonyl)-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / Et₃N / CH₂Cl₂ / 18 h / Heating

2: 96 percent / KOH / methanol / 1.5 h / Heating

With potassium hydroxide; triethylamine; In methanol; dichloromethane;
DOI:10.1039/b311520h