Technology Process of C67H71N4O11PS
There total 13 articles about C67H71N4O11PS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrachloromethane;
Inert atmosphere;
DOI:10.1021/op500042u
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dichloromethane / 1.5 h / 15 - 25 °C / Inert atmosphere; Large scale; Green chemistry
2: phosphorous acid; pivaloyl chloride / dichloromethane / 2 h / 20 - 25 °C / Inert atmosphere; Large scale; Green chemistry
3: pivaloyl chloride; pyridine / Inert atmosphere
4: tetrachloromethane / Inert atmosphere
With
pyridine; tetrachloromethane; pivaloyl chloride; phosphorous acid;
In
dichloromethane;
4: |Atherton-Todd Synthesis;
DOI:10.1021/op500042u
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dichloromethane / 1 h / 20 - 25 °C / Inert atmosphere; Large scale; Green chemistry
2: dichloromethane / 1.5 h / 15 - 25 °C / Inert atmosphere; Large scale; Green chemistry
3: phosphorous acid; pivaloyl chloride / dichloromethane / 2 h / 20 - 25 °C / Inert atmosphere; Large scale; Green chemistry
4: pivaloyl chloride; pyridine / Inert atmosphere
5: tetrachloromethane / Inert atmosphere
With
pyridine; tetrachloromethane; pivaloyl chloride; phosphorous acid;
In
dichloromethane;
5: |Atherton-Todd Synthesis;
DOI:10.1021/op500042u