dimethylphenylphosphonium pentachloro(dimethylphenylphosphine)niobate(IV)

Base Information

Chemical Name:dimethylphenylphosphonium pentachloro(dimethylphenylphosphine)niobate(IV)
CAS No.:130638-02-7
Molecular Formula:C₈H₁₁Cl₅NbP*C₈H₁₁P*H
Molecular Weight:547.478
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Chemical Property of dimethylphenylphosphonium pentachloro(dimethylphenylphosphine)niobate(IV)

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Technology Process of dimethylphenylphosphonium pentachloro(dimethylphenylphosphine)niobate(IV)

There total 1 articles about dimethylphenylphosphonium pentachloro(dimethylphenylphosphine)niobate(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

: 10026-12-7
niobium pentachloride

: 672-66-2
Dimethyl(phenyl)phosphine

: 130638-02-7
dimethylphenylphosphonium pentachloro(dimethylphenylphosphine)niobate(IV)

Guidance literature:: With Na/Hg; In toluene; reducing NbCl5 in toluene with one equivalent of Na/Hg in the presence of P(CH3)2(C6H5); filtration, evapn. to dryness, dissolving residue in CH2Cl2, crystn. on placing a layer of hexane over this soln.;