(4R)-7-bromo-2ξ-phenyl-(3at,13at)-4,5,13,13a-tetrahydro-3aH-4r,13c-epioxido-[1,3]dioxolo[4,5-e]pyrimido[5',4':4,5]pyrrolo[2,1-b][1,3]oxazocin-8-ylamine

Base Information

• Chemical Name: (4R)-7-bromo-2ξ-phenyl-(3at,13at)-4,5,13,13a-tetrahydro-3aH-4r,13c-epioxido-[1,3]dioxolo[4,5-e]pyrimido[5',4':4,5]pyrrolo[2,1-b][1,3]oxazocin-8-ylamine
• CAS No.: 52471-54-2
• Molecular Formula: C₁₈H₁₅BrN₄O₄
• Molecular Weight: 431.245

Synonyms:

Chemical Property of (4R)-7-bromo-2ξ-phenyl-(3at,13at)-4,5,13,13a-tetrahydro-3aH-4r,13c-epioxido-[1,3]dioxolo[4,5-e]pyrimido[5',4':4,5]pyrrolo[2,1-b][1,3]oxazocin-8-ylamine

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Technology Process of (4R)-7-bromo-2ξ-phenyl-(3at,13at)-4,5,13,13a-tetrahydro-3aH-4r,13c-epioxido-[1,3]dioxolo[4,5-e]pyrimido[5',4':4,5]pyrrolo[2,1-b][1,3]oxazocin-8-ylamine

There total 1 articles about (4R)-7-bromo-2ξ-phenyl-(3at,13at)-4,5,13,13a-tetrahydro-3aH-4r,13c-epioxido-[1,3]dioxolo[4,5-e]pyrimido[5',4':4,5]pyrrolo[2,1-b][1,3]oxazocin-8-ylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(4-amino-pyrrolo[2,3-d]pyrimidin-7-yl)-O2,O3-benzylidene-β-D-1-deoxy-ribofuranose (51008-63-0) → (4R)-7-bromo-2ξ-phenyl-(3at,13at)-4,5,13,13a-tetrahydro-3aH-4r,13c-epioxido-[1,3]dioxolo[4,5-e]pyrimido[5',4':4,5]pyrrolo[2,1-b][1,3]oxazocin-8-ylamine (52471-54-2,52520-84-0)

Guidance literature:

With N-Bromosuccinimide; barium carbonate; In tetrachloromethane;

DOI:10.1246/bcsj.47.417

Reference yield:

(4R)-7-bromo-2ξ-phenyl-(3at,13at)-4,5,13,13a-tetrahydro-3aH-4r,13c-epioxido-[1,3]dioxolo[4,5-e]pyrimido[5',4':4,5]pyrrolo[2,1-b][1,3]oxazocin-8-ylamine (52471-54-2,52520-84-0) → (4R)-2ξ-phenyl-(3at,13at)-4,5,13,13a-tetrahydro-3aH-4r,13c-epioxido-[1,3]dioxolo[4,5-e]pyrimido[5',4':4,5]pyrrolo[2,1-b][1,3]oxazocin-8-ylamine (52471-56-4)

Guidance literature:

With hydrogen; sodium acetate; palladium on activated charcoal; In ethanol;

DOI:10.1246/bcsj.47.417

upstream raw materials:

1-(4-amino-pyrrolo[2,3-d]pyrimidin-7-yl)-O²,O³-benzylidene-β-D-1-deoxy-ribofuranose

Downstream raw materials:

(4R)-2ξ-phenyl-(3at,13at)-4,5,13,13a-tetrahydro-3aH-4r,13c-epioxido-[1,3]dioxolo[4,5-e]pyrimido[5',4':4,5]pyrrolo[2,1-b][1,3]oxazocin-8-ylamine

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