((thiophosphinoyl)(trimethylsilyl)methanido)bis(2,6-dimethylphenyl isocyanide)rhodium

Base Information

Chemical Name:((thiophosphinoyl)(trimethylsilyl)methanido)bis(2,6-dimethylphenyl isocyanide)rhodium
CAS No.:1370329-12-6
Molecular Formula:C₃₄H₃₈N₂PRhSSi
Molecular Weight:668.72
Hs Code.:

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Chemical Property of ((thiophosphinoyl)(trimethylsilyl)methanido)bis(2,6-dimethylphenyl isocyanide)rhodium

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Technology Process of ((thiophosphinoyl)(trimethylsilyl)methanido)bis(2,6-dimethylphenyl isocyanide)rhodium

There total 1 articles about ((thiophosphinoyl)(trimethylsilyl)methanido)bis(2,6-dimethylphenyl isocyanide)rhodium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 1370329-10-4
(thiophosphinoyl)((trimethylsilyl)methanido)(1,5-cyclooctadiene)rhodium

: 1370329-12-6
((thiophosphinoyl)(trimethylsilyl)methanido)bis(2,6-dimethylphenyl isocyanide)rhodium

Guidance literature:: In toluene; Ar or N2, Schlenk and glovebox technique; to soln. of Rh-complex isocyanide added under N2, stirred for 15 min; solvent evapd. (vac.), petroleum ether added (N2), ppt. centrifuged, washed twice (petroleum ether);
DOI:10.1002/ejic.201101073