Cp*Ir(η2-C6H4)(PMe3)

Base Information

Chemical Name:Cp*Ir(η2-C6H4)(PMe3)
CAS No.:476407-15-5
Molecular Formula:C₁₉H₂₈IrP
Molecular Weight:479.625
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cp*Ir(η2-C6H4)(PMe3)

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Technology Process of Cp*Ir(η2-C6H4)(PMe3)

There total 1 articles about Cp*Ir(η2-C6H4)(PMe3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 109-72-8,29786-93-4
n-butyllithium

: 476407-14-4
C₅(CH₃)5IrC₆FH₄(P(CH₃)3)H

: 114378-46-0
(η5-C5Me5)Ir(PMe3)(C6H5)n-C4H9

: 476407-15-5
Cp*Ir(η2-C6H4)(PMe3)

Guidance literature:: In hexane; (N2); addn. of a soln. of lithium compd. in hexane to a soln. of iridiumcomplex in hexane, stirring for 4 h at room temp., cooling to 0° C, addn. of MeOH; evapn., extn. with hexanes, filtration, slow evapn.; elem. anal.;
DOI:10.1021/om0204787

Reference yield: 95.0%

: 476407-15-5
Cp*Ir(η2-C6H4)(PMe3)

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 528868-49-7
Cp*Ir(2-C₆IH₄)(PMe₃)I

Guidance literature:: In hexane; under N2 atm. to soln. Ir complexin hexane I2 in hexane was added dropwise; ppt. was filtered and crystd. from toluene; elem. anal.;
DOI:10.1021/om030048w