O⁴-(6-amino-2-benzyloxycarbonylamino-N⁶,O⁴-carbonyl-O³-(Ξ)-tetrahydropyran-2-yl-α-D-2,6-dideoxy-glucopyranosyl)-N³-benzyloxycarbonyl-N¹,O⁶-carbonyl-O⁵-(tri-O-benzoyl-β-D-ribofuranosyl)-1D-2-deoxy-streptamine

Base Information

• Chemical Name: O⁴-(6-amino-2-benzyloxycarbonylamino-N⁶,O⁴-carbonyl-O³-(Ξ)-tetrahydropyran-2-yl-α-D-2,6-dideoxy-glucopyranosyl)-N³-benzyloxycarbonyl-N¹,O⁶-carbonyl-O⁵-(tri-O-benzoyl-β-D-ribofuranosyl)-1D-2-deoxy-streptamine
• CAS No.: 66787-87-9
• Molecular Formula: C₆₁H₆₂N₄O₂₀
• Molecular Weight: 1171.18

Synonyms:

Chemical Property of O⁴-(6-amino-2-benzyloxycarbonylamino-N⁶,O⁴-carbonyl-O³-(Ξ)-tetrahydropyran-2-yl-α-D-2,6-dideoxy-glucopyranosyl)-N³-benzyloxycarbonyl-N¹,O⁶-carbonyl-O⁵-(tri-O-benzoyl-β-D-ribofuranosyl)-1D-2-deoxy-streptamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O⁴-(6-amino-2-benzyloxycarbonylamino-N⁶,O⁴-carbonyl-O³-(Ξ)-tetrahydropyran-2-yl-α-D-2,6-dideoxy-glucopyranosyl)-N³-benzyloxycarbonyl-N¹,O⁶-carbonyl-O⁵-(tri-O-benzoyl-β-D-ribofuranosyl)-1D-2-deoxy-streptamine

There total 4 articles about O⁴-(6-amino-2-benzyloxycarbonylamino-N⁶,O⁴-carbonyl-O³-(Ξ)-tetrahydropyran-2-yl-α-D-2,6-dideoxy-glucopyranosyl)-N³-benzyloxycarbonyl-N¹,O⁶-carbonyl-O⁵-(tri-O-benzoyl-β-D-ribofuranosyl)-1D-2-deoxy-streptamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-dihydro-2H-pyran (110-87-2) → O4-(6-amino-2-benzyloxycarbonylamino-N6,O4-carbonyl-O3-(Ξ)-tetrahydropyran-2-yl-α-D-2,6-dideoxy-glucopyranosyl)-N3-benzyloxycarbonyl-N1,O6-carbonyl-O5-(tri-O-benzoyl-β-D-ribofuranosyl)-1D-2-deoxy-streptamine (66787-87-9)

Guidance literature:

Multi-step reaction with 2 steps

1: TsOH / dimethylformamide

2: Hg(CN)2, Drierite / CHCl₃

With calcium sulfate; mercury(II) cyanide; toluene-4-sulfonic acid; In chloroform; N,N-dimethyl-formamide;

DOI:10.1021/jo00411a014

Reference yield:

3,2'-di-N-benzyloxycarbonyl-1,6:6',4'-N,O-carbonyl-neamine (66787-82-4) → O4-(6-amino-2-benzyloxycarbonylamino-N6,O4-carbonyl-O3-(Ξ)-tetrahydropyran-2-yl-α-D-2,6-dideoxy-glucopyranosyl)-N3-benzyloxycarbonyl-N1,O6-carbonyl-O5-(tri-O-benzoyl-β-D-ribofuranosyl)-1D-2-deoxy-streptamine (66787-87-9)

Guidance literature:

Multi-step reaction with 2 steps

1: TsOH / dimethylformamide

2: Hg(CN)2, Drierite / CHCl₃

With calcium sulfate; mercury(II) cyanide; toluene-4-sulfonic acid; In chloroform; N,N-dimethyl-formamide;

DOI:10.1021/jo00411a014

Reference yield:

N,N',N'',N'''-tetra(benzyloxycarbonyl)neamine (22854-75-7) → O4-(6-amino-2-benzyloxycarbonylamino-N6,O4-carbonyl-O3-(Ξ)-tetrahydropyran-2-yl-α-D-2,6-dideoxy-glucopyranosyl)-N3-benzyloxycarbonyl-N1,O6-carbonyl-O5-(tri-O-benzoyl-β-D-ribofuranosyl)-1D-2-deoxy-streptamine (66787-87-9)

Guidance literature:

Multi-step reaction with 3 steps

1: NaH / dimethylformamide

2: TsOH / dimethylformamide

3: Hg(CN)2, Drierite / CHCl₃

With calcium sulfate; mercury(II) cyanide; sodium hydride; toluene-4-sulfonic acid; In chloroform; N,N-dimethyl-formamide;

DOI:10.1021/jo00411a014

upstream raw materials:

O⁴-(6-amino-2-benzyloxycarbonylamino-N⁶,O⁴-carbonyl-O³-(Ξ)-tetrahydropyran-2-yl-α-D-2,6-dideoxy-glucopyranosyl)-N³-benzyloxycarbonyl-N¹,O⁶-carbonyl-1D-2-deoxy-streptamine

β-D-2,3,5-tri-O-benzoylribofuranosyl chloride

3,4-dihydro-2H-pyran

3,2'-di-N-benzyloxycarbonyl-1,6:6',4'-N,O-carbonyl-neamine

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