Technology Process of nitrogen sulfide
There total 6 articles about nitrogen sulfide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
gaseous matrix;
a 2% mixture of N2 in Ar passed through discharge tube seeded with sulfur vapor in equilibrium with the solid at 25°C-115°C; trappening in solid Ar; not isolated, detected by IR; influence of annealing on product-distribution;
DOI:10.1021/ja00027a012
- Guidance literature:
-
In
neat (no solvent);
byproducts: benzonitrile; flash vac. pyrolysis in unpacked quartz tubes at temps. from 200 - 700°C (1E-4 mbar);; isolating the products in Ar or Xe matrices at 12 - 20 K or neat at 77 K;
DOI:10.1021/j100184a010
- Guidance literature:
-
In
neat (no solvent);
byproducts: benzonitrile-d5; flash vac. pyrolysis in unpacked quartz tubes at temps. from 200 - 700°C (1E-4 mbar); isolating the products in Ar or Xe matrices at 12 - 20 K or neat at 77 K;
DOI:10.1021/j100184a010
