C₂₇H₄₅NO₃

Base Information

Chemical Name:C₂₇H₄₅NO₃
CAS No.:1429195-17-4
Molecular Formula:C₂₇H₄₅NO₃
Molecular Weight:431.659
Hs Code.:

C<sub>27</sub>H<sub>45</sub>NO<sub>3</sub>

Synonyms:

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Chemical Property of C₂₇H₄₅NO₃

Chemical Property:

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Technology Process of C₂₇H₄₅NO₃

There total 7 articles about C₂₇H₄₅NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79299-29-9
(E)-1-phenyl-1,5-hexadien-3-ol

: 1429195-17-4
C₂₇H₄₅NO₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: titanium(IV) isopropylate; diethyl (2S,3S)-tartrate / dichloromethane / 0.25 h / -20 °C

1.2: 3 h / -20 °C / Molecular sieve

2.1: sodium azide / acetonitrile / Molecular sieve

3.1: pyridine; dmap / 3 h / 20 °C / Inert atmosphere

4.1: sodium periodate; 2,6-dimethylpyridine; osmium(VIII) oxide / 1,4-dioxane; water; isopropyl alcohol / 6 h / 20 °C

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -15 °C

5.2: 3.25 h / -15 - 20 °C

6.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 3 h / 20 °C

7.1: pyridine / dichloromethane / 2 h / 20 °C

With pyridine; 2,6-dimethylpyridine; titanium(IV) isopropylate; dmap; sodium periodate; osmium(VIII) oxide; n-butyllithium; sodium azide; diethyl (2S,3S)-tartrate; palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; water; ethyl acetate; isopropyl alcohol; acetonitrile; 5.1: |Wittig Olefination / 5.2: |Wittig Olefination;
DOI:10.1016/j.tet.2013.03.057

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 1429195-17-4
C₂₇H₄₅NO₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrahydrofuran / 2.75 h / 0 - 20 °C

2.1: titanium(IV) isopropylate; diethyl (2S,3S)-tartrate / dichloromethane / 0.25 h / -20 °C

2.2: 3 h / -20 °C / Molecular sieve

3.1: sodium azide / acetonitrile / Molecular sieve

4.1: pyridine; dmap / 3 h / 20 °C / Inert atmosphere

5.1: sodium periodate; 2,6-dimethylpyridine; osmium(VIII) oxide / 1,4-dioxane; water; isopropyl alcohol / 6 h / 20 °C

6.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -15 °C

6.2: 3.25 h / -15 - 20 °C

7.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 3 h / 20 °C

8.1: pyridine / dichloromethane / 2 h / 20 °C

With pyridine; 2,6-dimethylpyridine; titanium(IV) isopropylate; dmap; sodium periodate; osmium(VIII) oxide; n-butyllithium; sodium azide; diethyl (2S,3S)-tartrate; palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; water; ethyl acetate; isopropyl alcohol; acetonitrile; 6.1: |Wittig Olefination / 6.2: |Wittig Olefination;
DOI:10.1016/j.tet.2013.03.057

Reference yield:

: 1429195-14-1
C₁₆H₁₉N₃O₄

: 1429195-17-4
C₂₇H₄₅NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium periodate; 2,6-dimethylpyridine; osmium(VIII) oxide / 1,4-dioxane; water; isopropyl alcohol / 6 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -15 °C

2.2: 3.25 h / -15 - 20 °C

3.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 3 h / 20 °C

4.1: pyridine / dichloromethane / 2 h / 20 °C

With pyridine; 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; n-butyllithium; palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; water; ethyl acetate; isopropyl alcohol; 2.1: |Wittig Olefination / 2.2: |Wittig Olefination;
DOI:10.1016/j.tet.2013.03.057