Technology Process of C20H20N2O6
There total 20 articles about C20H20N2O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: NaHCO3 / CH2Cl2; H2O / 1 h / Ambient temperature
2: LiOH / ethanol / 24 h / Ambient temperature
3: Et3N / tetrahydrofuran / 1.5 h / 0 °C
4: tetrahydrofuran / 2 h / 0 °C
5: 50 percent / N-bromosuccinimide (NBS) / CHCl3 / Ambient temperature
6: silver triflate / tetrahydrofuran; H2O / 0.5 h / Ambient temperature
With
lithium hydroxide; N-Bromosuccinimide; silver trifluoromethanesulfonate; sodium hydrogencarbonate; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane; chloroform; water;
DOI:10.1021/ja00055a025
- Guidance literature:
-
Multi-step reaction with 6 steps
1: NaHCO3 / CH2Cl2; H2O / 1 h / Ambient temperature
2: LiOH / ethanol / 24 h / Ambient temperature
3: Et3N / tetrahydrofuran / 1.5 h / 0 °C
4: tetrahydrofuran / 2 h / 0 °C
5: 50 percent / N-bromosuccinimide (NBS) / CHCl3 / Ambient temperature
6: silver triflate / tetrahydrofuran; H2O / 0.5 h / Ambient temperature
With
lithium hydroxide; N-Bromosuccinimide; silver trifluoromethanesulfonate; sodium hydrogencarbonate; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane; chloroform; water;
DOI:10.1021/ja00055a025
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Et3N / tetrahydrofuran / 1.5 h / 0 °C
2: tetrahydrofuran / 2 h / 0 °C
3: 50 percent / N-bromosuccinimide (NBS) / CHCl3 / Ambient temperature
4: silver triflate / tetrahydrofuran; H2O / 0.5 h / Ambient temperature
With
N-Bromosuccinimide; silver trifluoromethanesulfonate; triethylamine;
In
tetrahydrofuran; chloroform; water;
DOI:10.1021/ja00055a025