C₂₄H₄₃NO₅Si₂

Base Information

Chemical Name:C₂₄H₄₃NO₅Si₂
CAS No.:1364927-28-5
Molecular Formula:C₂₄H₄₃NO₅Si₂
Molecular Weight:481.78
Hs Code.:

C<sub>24</sub>H<sub>43</sub>NO<sub>5</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₂₄H₄₃NO₅Si₂

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Technology Process of C₂₄H₄₃NO₅Si₂

There total 8 articles about C₂₄H₄₃NO₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₅₁NO₇Si₂

: 1364927-28-5
C₂₄H₄₃NO₅Si₂

Guidance literature:: With palladium 10% on activated carbon; hydrogen; triethylamine; In ethyl acetate; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.201102066

Reference yield:

: C₃₂H₄₉NO₆Si₂

: 1364927-28-5
C₂₄H₄₃NO₅Si₂

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere

2: sodium triacetoxyborohydride; acetic acid / acetonitrile / 1 h / 0 °C / Inert atmosphere

3: pyridine / 2.15 h / 20 °C / Inert atmosphere

4: palladium 10% on activated carbon; hydrogen; triethylamine / ethyl acetate / 1 h / 20 °C / Inert atmosphere

With pyridine; palladium 10% on activated carbon; sodium triacetoxyborohydride; tetrabutyl ammonium fluoride; hydrogen; acetic acid; triethylamine; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201102066

Reference yield:

: 1241725-14-3
C₁₇H₃₆O₃Si₂

: 1364927-28-5
C₂₄H₄₃NO₅Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: tributyl-amine; triphenyl-arsane; palladium diacetate / N,N-dimethyl-formamide / 15 h / 20 - 70 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere

3: sodium triacetoxyborohydride; acetic acid / acetonitrile / 1 h / 0 °C / Inert atmosphere

4: pyridine / 2.15 h / 20 °C / Inert atmosphere

5: palladium 10% on activated carbon; hydrogen; triethylamine / ethyl acetate / 1 h / 20 °C / Inert atmosphere

With pyridine; tributyl-amine; triphenyl-arsane; palladium 10% on activated carbon; sodium triacetoxyborohydride; tetrabutyl ammonium fluoride; hydrogen; palladium diacetate; acetic acid; triethylamine; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; 1: Heck reaction;
DOI:10.1002/chem.201102066