(E)-α-santalal

Base Information

Chemical Name:(E)-α-santalal
CAS No.:19903-70-9
Molecular Formula:C₁₅H₂₂O
Molecular Weight:218.339
Hs Code.:

Synonyms:

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Chemical Property of (E)-α-santalal

Chemical Property:

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Technology Process of (E)-α-santalal

There total 11 articles about (E)-α-santalal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: (Z)-5-(dimethyltricyclo<2.2.1.0^2,6>hept-3-yl)-2-methylpent-2-enal

: 13827-97-9,19903-70-9,73307-64-9
(E)-5-(2,3-dimethyltricyclo<2.2.1.0^2,6>hept-3-yl)-2-methylpent-2-enal

Guidance literature:: With benzoic acid; In chloroform; at 100 ℃; for 24h;
DOI:10.1016/S0040-4039(00)73929-3

Reference yield:

: 7-((Z)-4-Methoxy-pent-3-enyl)-1,7-dimethyl-tricyclo[2.2.1.0^2,6]heptane

: 13827-97-9,19903-70-9,73307-64-9
(E)-α-santalal

Guidance literature:: With sodium acetate; pyridinium chlorochromate; In dichloromethane; for 20h; Ambient temperature;
DOI:10.1021/jo00245a012

Reference yield:

: 52645-83-7,95910-71-7
8-bromotricyclene

: 13827-97-9,19903-70-9,73307-64-9
(E)-5-(2,3-dimethyltricyclo<2.2.1.0^2,6>hept-3-yl)-2-methylpent-2-enal

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / K-t-BuO, BuLi / tetrahydrofuran / 0.5 h / -75 °C

2: 46 percent / K-t-BuO, BuLi, fluorodimethoxyborane diethyl etherate, 30 percent aq. hydrogen peroxide / tetrahydrofuran / 1 h / 25 °C

3: 96 percent / MnO₂ / hexane / 24 h / 25 °C

4: 95 percent / benzoic acid / CHCl₃ / 24 h / 100 °C

With manganese(IV) oxide; n-butyllithium; fluorodimethoxyborane diethyl etherate; potassium tert-butylate; dihydrogen peroxide; benzoic acid; In tetrahydrofuran; hexane; chloroform;
DOI:10.1016/S0040-4039(00)73929-3