Technology Process of C31H50O5Si
There total 5 articles about C31H50O5Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 2 steps
1: bis(cyclopentadienyl)titanium dichloride; zinc / tetrahydrofuran / 1 h / 20 °C
2: lanthanum(lll) triflate / toluene / 0.75 h / 20 °C
With
bis(cyclopentadienyl)titanium dichloride; zinc; lanthanum(lll) triflate;
In
tetrahydrofuran; toluene;
DOI:10.1002/ejoc.201001104
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tert.-butylhydroperoxide; selenium(IV) oxide / dichloromethane
2: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -20 °C / Molecular sieve
3: 1H-imidazole / N,N-dimethyl-formamide
4: bis(cyclopentadienyl)titanium dichloride; zinc / tetrahydrofuran / 1 h / 20 °C
5: lanthanum(lll) triflate / toluene / 0.75 h / 20 °C
With
1H-imidazole; titanium(IV) isopropylate; tert.-butylhydroperoxide; selenium(IV) oxide; bis(cyclopentadienyl)titanium dichloride; diethyl (2R,3R)-tartrate; zinc; lanthanum(lll) triflate;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;
2: Sharpless epoxidation;
DOI:10.1002/ejoc.201001104