(3RS,4SR)-1--3-phenoxyacetamido-4-prop-2-enylazetidin-2-one

Base Information

Chemical Name:(3RS,4SR)-1--3-phenoxyacetamido-4-prop-2-enylazetidin-2-one
CAS No.:112213-45-3
Molecular Formula:C₂₃H₂₄N₂O₆
Molecular Weight:424.453
Hs Code.:

(3RS,4SR)-1-<benzyloxycarbonyl(hydroxy)methyl>-3-phenoxyacetamido-4-prop-2-enylazetidin-2-one

Synonyms:

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Chemical Property of (3RS,4SR)-1--3-phenoxyacetamido-4-prop-2-enylazetidin-2-one

Chemical Property:

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Technology Process of (3RS,4SR)-1--3-phenoxyacetamido-4-prop-2-enylazetidin-2-one

There total 9 articles about (3RS,4SR)-1--3-phenoxyacetamido-4-prop-2-enylazetidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 52709-42-9
benzylglyoxylate

: 82792-77-6,87144-61-4,103366-39-8,103366-40-1,131177-04-3,131177-06-5
(3RS,4SR)-3-phenoxyacetamido-4-prop-2-enylazetidin-2-one

: 112213-45-3
(3RS,4SR)-1--3-phenoxyacetamido-4-prop-2-enylazetidin-2-one

Guidance literature:: In benzene; for 1h; Heating;

Reference yield:

: 112213-44-2
(3RS,4SR)-4-<3-hydroxyprop-1-ynyl>-1-(4-methoxymethoxyphenyl)-3-phenoxyacetamidoazetidin-2-one

: 112213-45-3
(3RS,4SR)-1--3-phenoxyacetamido-4-prop-2-enylazetidin-2-one

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / H₂ / 10percent Pd-C / dioxane / 6.5 h

2: 97 percent / triethylamine / CH₂Cl₂ / 5 h / 0 °C

3: 1.) o-nitrophenylselenocyanate, sodium brorhydride; 2.) m-chloroperbenzoic acid / 1.) dimethoxyethane rt., 24 h; 2.) 2 d

4: 64 percent / CH₂Cl₂

5: 91 percent / benzene / 1 h / Heating

With sodium tetrahydroborate; ortho-nitrophenyl selenocyanate; hydrogen; triethylamine; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In 1,4-dioxane; dichloromethane; benzene;

Reference yield:

: (3RS,4SR)-3-azido-4-<3-diphenyl-t-butylsilyloxyprop-1-ynyl>-1-(4-methoxymethoxyphenyl)azetidin-2-one

: 112213-45-3
(3RS,4SR)-1--3-phenoxyacetamido-4-prop-2-enylazetidin-2-one

Guidance literature:: Multi-step reaction with 8 steps

1: triethylamine, hydrogensulphide / CH₂Cl₂ / 0 °C

2: CH₂Cl₂

3: 92 percent / tetraethylammonium fluride dihydrate / tetrahydrofuran / 20 h

4: 80 percent / H₂ / 10percent Pd-C / dioxane / 6.5 h

5: 97 percent / triethylamine / CH₂Cl₂ / 5 h / 0 °C

6: 1.) o-nitrophenylselenocyanate, sodium brorhydride; 2.) m-chloroperbenzoic acid / 1.) dimethoxyethane rt., 24 h; 2.) 2 d

7: 64 percent / CH₂Cl₂

8: 91 percent / benzene / 1 h / Heating

With sodium tetrahydroborate; ortho-nitrophenyl selenocyanate; hydrogen sulfide; hydrogen; tetraethylammonium fluoride; triethylamine; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; dichloromethane; benzene;