Technology Process of C10H10N2O2
There total 4 articles about C10H10N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: [bis(acetoxy)iodo]benzene; potassium carbonate / dimethyl sulfoxide / 24 h / 20 °C / Inert atmosphere
2.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 20 - 55 °C / Inert atmosphere
2.2: 3 h / 20 °C
3.1: pyridine hydrochloride / 5 h / 200 °C / Inert atmosphere
With
[bis(acetoxy)iodo]benzene; pyridine hydrochloride; sodium hydride; potassium carbonate;
In
tetrahydrofuran; dimethyl sulfoxide; mineral oil;
DOI:10.1002/chem.201001921
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: dichloromethane / 0.5 h / 0 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: [bis(acetoxy)iodo]benzene; potassium carbonate / dimethyl sulfoxide / 24 h / 20 °C / Inert atmosphere
3.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 20 - 55 °C / Inert atmosphere
3.2: 3 h / 20 °C
4.1: pyridine hydrochloride / 5 h / 200 °C / Inert atmosphere
With
[bis(acetoxy)iodo]benzene; pyridine hydrochloride; sodium hydride; potassium carbonate;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; mineral oil;
DOI:10.1002/chem.201001921