C₂₂H₃₈OSi

Base Information

Chemical Name:C₂₂H₃₈OSi
CAS No.:1350626-70-8
Molecular Formula:C₂₂H₃₈OSi
Molecular Weight:346.629
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₃₈OSi

Chemical Property:

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Technology Process of C₂₂H₃₈OSi

There total 7 articles about C₂₂H₃₈OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₆H₄₆OSi₂

: 1350626-70-8
C₂₂H₃₈OSi

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; at 20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1021/ja209553f

Reference yield:

: 1172850-67-7
C₁₇H₂₂O₂

: 1350626-70-8
C₂₂H₃₈OSi

Guidance literature:: Multi-step reaction with 6 steps

1: toluene-4-sulfonic acid / methanol / 2 h / 20 °C / Inert atmosphere

2: manganese(IV) oxide / diethyl ether / 8 h / 20 °C / Inert atmosphere

3: tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

4: 1H-imidazole / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere

5: platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / 5,5-dimethyl-1,3-cyclohexadiene / 1 h / 80 °C / Inert atmosphere

6: tetrabutyl ammonium fluoride / tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene / 0.25 h / 20 °C / Inert atmosphere

With 1H-imidazole; manganese(IV) oxide; platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; 5,5-dimethyl-1,3-cyclohexadiene; diethyl ether;
DOI:10.1021/ja209553f

Reference yield:

: 1350626-61-7
3f

: 1350626-70-8
C₂₂H₃₈OSi

Guidance literature:: Multi-step reaction with 2 steps

1: platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / 5,5-dimethyl-1,3-cyclohexadiene / 1 h / 80 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene / 0.25 h / 20 °C / Inert atmosphere

With platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; tetrabutyl ammonium fluoride; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene;
DOI:10.1021/ja209553f