((3aR)-8c-hydroxy-2,2,5c,12-tetramethyl-11-oxo-(3ar,6at,7ac,9ac,12ac,12bt,13atC¹)-decahydro-[1,3]dioxolo[4''',5''':3'',4'']pyrano[3'',2'':5',6'][1,4]dioxino[2',3':5,6]benzo[1,2-d]oxazol-9t-yl)-methyl-carbamic acid benzyl ester

Base Information

• Chemical Name: ((3aR)-8c-hydroxy-2,2,5c,12-tetramethyl-11-oxo-(3ar,6at,7ac,9ac,12ac,12bt,13atC¹)-decahydro-[1,3]dioxolo[4''',5''':3'',4'']pyrano[3'',2'':5',6'][1,4]dioxino[2',3':5,6]benzo[1,2-d]oxazol-9t-yl)-methyl-carbamic acid benzyl ester
• CAS No.: 67421-56-1
• Molecular Formula: C₂₆H₃₄N₂O₁₀
• Molecular Weight: 534.563

Synonyms:

Chemical Property of ((3aR)-8c-hydroxy-2,2,5c,12-tetramethyl-11-oxo-(3ar,6at,7ac,9ac,12ac,12bt,13atC¹)-decahydro-[1,3]dioxolo[4''',5''':3'',4'']pyrano[3'',2'':5',6'][1,4]dioxino[2',3':5,6]benzo[1,2-d]oxazol-9t-yl)-methyl-carbamic acid benzyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ((3aR)-8c-hydroxy-2,2,5c,12-tetramethyl-11-oxo-(3ar,6at,7ac,9ac,12ac,12bt,13atC¹)-decahydro-[1,3]dioxolo[4''',5''':3'',4'']pyrano[3'',2'':5',6'][1,4]dioxino[2',3':5,6]benzo[1,2-d]oxazol-9t-yl)-methyl-carbamic acid benzyl ester

There total 2 articles about ((3aR)-8c-hydroxy-2,2,5c,12-tetramethyl-11-oxo-(3ar,6at,7ac,9ac,12ac,12bt,13atC¹)-decahydro-[1,3]dioxolo[4''',5''':3'',4'']pyrano[3'',2'':5',6'][1,4]dioxino[2',3':5,6]benzo[1,2-d]oxazol-9t-yl)-methyl-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N'-dimethyl-N,N'-((3aR)-8c,10t-dihydroxy-2,2,5c-trimethyl-(3ar,6at,7ac,11at,12atO1)-octahydro-benzo[b][1,3]dioxolo[4',5':3,4]pyrano[2,3-e][1,4]dioxine-9t,11t-diyl)-bis-carbamic acid dibenzyl ester (58515-30-3,58560-41-1,67462-78-6,68906-66-1) → ((3aR)-8c-hydroxy-2,2,5c,12-tetramethyl-11-oxo-(3ar,6at,7ac,9ac,12ac,12bt,13atC1)-decahydro-[1,3]dioxolo[4''',5''':3'',4'']pyrano[3'',2'':5',6'][1,4]dioxino[2',3':5,6]benzo[1,2-d]oxazol-9t-yl)-methyl-carbamic acid benzyl ester (67421-56-1,67462-81-1)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 24h;

DOI:10.1021/jo00416a021

Reference yield:

N,N'-dimethyl-N,N'-((3aR)-8t,10c-dihydroxy-2,2,5c-trimethyl-(3ar,6at,7at,11ac,12atO1)-octahydro-benzo[b][1,3]dioxolo[4',5':3,4]pyrano[2,3-e][1,4]dioxine-9c,11c-diyl)-bis-carbamic acid dibenzyl ester (58515-30-3,58560-41-1,67462-78-6,68906-66-1) → ((3aR)-8t-hydroxy-2,2,5c,12-tetramethyl-11-oxo-(3ar,6at,7at,9at,12at,12bc,13atO1)-decahydro-[1,3]dioxolo[3''',4''':3'',4'']pyrano[3'',2'':5',6'][1,4]dioxino[2',3':5,6]benzo[1,2-d]oxazol-9c-yl)-methyl-carbamic acid benzyl ester (67421-56-1,67462-81-1)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 95 ℃; for 4h;

DOI:10.1021/jo00416a021

Reference yield:

((3aR)-8c-hydroxy-2,2,5c,12-tetramethyl-11-oxo-(3ar,6at,7ac,9ac,12ac,12bt,13atC1)-decahydro-[1,3]dioxolo[4''',5''':3'',4'']pyrano[3'',2'':5',6'][1,4]dioxino[2',3':5,6]benzo[1,2-d]oxazol-9t-yl)-methyl-carbamic acid benzyl ester (67421-56-1,67462-81-1) → ((3aS)-5c,10t,10a-trihydroxy-1,8c-dimethyl-2-oxo-(3ar,5ac,6at,10at,11at,11bc)-dodecahydro-pyrano[3'',2'':5',6'][1,4]dioxino[2',3':5,6]benzo[1,2-d]oxazol-4t-yl)-methyl-carbamic acid benzyl ester (67421-59-4)

Guidance literature:

With hydrogenchloride; In methanol; for 0.416667h; Heating;

DOI:10.1021/jo00416a021

upstream raw materials:

N,N'-dimethyl-N,N'-((3aR)-8t,10c-dihydroxy-2,2,5c-trimethyl-(3ar,6at,7at,11ac,12atO¹)-octahydro-benzo[b][1,3]dioxolo[4',5':3,4]pyrano[2,3-e][1,4]dioxine-9c,11c-diyl)-bis-carbamic acid dibenzyl ester

N,N'-dimethyl-N,N'-((3aR)-8c,10t-dihydroxy-2,2,5c-trimethyl-(3ar,6at,7ac,11at,12atO¹)-octahydro-benzo[b][1,3]dioxolo[4',5':3,4]pyrano[2,3-e][1,4]dioxine-9t,11t-diyl)-bis-carbamic acid dibenzyl ester

Downstream raw materials:

((3aR)-8t-benzoyloxy-2,2,5c,12-tetramethyl-11-oxo-(3ar,6at,7at,9at,12at,12bc,13atO¹)-decahydro-[1,3]dioxolo[3''',4''':3'',4'']pyrano[3'',2'':5',6'][1,4]dioxino[2',3':5,6]benzo[1,2-d]oxazol-9c-yl)-methyl-carbamic acid benzyl ester

((3aS)-5c,10t,10a-trihydroxy-1,8c-dimethyl-2-oxo-(3ar,5ac,6at,10at,11at,11bc)-dodecahydro-pyrano[3'',2'':5',6'][1,4]dioxino[2',3':5,6]benzo[1,2-d]oxazol-4t-yl)-methyl-carbamic acid benzyl ester

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