C₅₂H₈₂N₁₂O₁₉S

Base Information

Chemical Name:C₅₂H₈₂N₁₂O₁₉S
CAS No.:1356410-08-6
Molecular Formula:C₅₂H₈₂N₁₂O₁₉S
Molecular Weight:1211.36
Hs Code.:

C<sub>52</sub>H<sub>82</sub>N<sub>12</sub>O<sub>19</sub>S

Synonyms:

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Chemical Property of C₅₂H₈₂N₁₂O₁₉S

Chemical Property:

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Technology Process of C₅₂H₈₂N₁₂O₁₉S

There total 10 articles about C₅₂H₈₂N₁₂O₁₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2468-56-6
1-iodo-5-hexyne

: 1356410-08-6
C₅₂H₈₂N₁₂O₁₉S

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 1.5 h / -78 - 0 °C

2.1: water; potassium hydroxide / methanol / Reflux

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

4.1: tetrahydrofuran; water / 0.25 h / 20 °C / pH 6.3 / aq. phosphate buffer

With dmap; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; hexane; dichloromethane; water;
DOI:10.1021/ja208009r

Reference yield:

: 101-41-7
benzeneacetic acid methyl ester

: 1356410-08-6
C₅₂H₈₂N₁₂O₁₉S

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 1.5 h / -78 - 0 °C

2.1: water; potassium hydroxide / methanol / Reflux

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

4.1: tetrahydrofuran; water / 0.25 h / 20 °C / pH 6.3 / aq. phosphate buffer

With dmap; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; hexane; dichloromethane; water;
DOI:10.1021/ja208009r

Reference yield:

: 1372710-96-7
C₁₅H₁₈O₂

: 1356410-08-6
C₅₂H₈₂N₁₂O₁₉S

Guidance literature:: Multi-step reaction with 3 steps

1: water; potassium hydroxide / methanol / Reflux

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

3: tetrahydrofuran; water / 0.25 h / 20 °C / pH 6.3 / aq. phosphate buffer

With dmap; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/ja208009r