trans-3,5-bis-p-cresoxycyclopentene

Base Information

• Chemical Name: trans-3,5-bis-p-cresoxycyclopentene
• CAS No.: 106550-27-0
• Molecular Formula: C₁₉H₂₀O₂
• Molecular Weight: 280.367

Synonyms:

Chemical Property of trans-3,5-bis-p-cresoxycyclopentene

Chemical Property:

Purity/Quality:

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Technology Process of trans-3,5-bis-p-cresoxycyclopentene

There total 2 articles about trans-3,5-bis-p-cresoxycyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclopentene (142-29-0) → trans-3,5-bis-p-cresoxycyclopentene (106550-27-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 25 percent / N-bromosuccinimide / CCl₄ / 1 h / Heating

2: 1.) KOH / 1.) 90percent ethanol, reflux, 1 h, 2.) 6 h

With potassium hydroxide; N-Bromosuccinimide; In tetrachloromethane;

Reference yield:

p-cresol (106-44-5) + trans-3,5-dibromocyclopentene (1890-04-6,17040-70-9,42086-51-1) → trans-3,5-bis-p-cresoxycyclopentene (106550-27-0)

Guidance literature:

With potassium hydroxide; Yield given. Multistep reaction; 1.) 90percent ethanol, reflux, 1 h, 2.) 6 h;

Reference yield: 62.0%

trans-3,5-bis-p-cresoxycyclopentene (106550-27-0) → 2-<5'-(p-cresoxy)-2'-cyclopentenyl>-p-cresol (106550-31-6)

Guidance literature:

With N,N-diethylaniline; for 10h; Heating;

upstream raw materials:

p-cresol

trans-3,5-dibromocyclopentene

cyclopentene

Downstream raw materials:

2-<5'-(p-cresoxy)-2'-cyclopentenyl>-p-cresol

7-Methyl-1-p-tolyloxy-3a,8b-dihydro-1H-benzo[b]cyclopenta[d]furan

12-Bromo-4-methyl-11-p-tolyloxy-8-oxa-tricyclo[7.2.1.0^2,7]dodeca-2,4,6-triene

3-bromo-1-(p-cresoxy)-2,3,3a,8b-tetrahydro-1H-cyclopentabenzofuran

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