HB(N,N'-diphenyl-1,2-ethylenediamine(-2H))

Base Information

• Chemical Name: HB(N,N'-diphenyl-1,2-ethylenediamine(-2H))
• CAS No.: 1365973-61-0
• Molecular Formula: C₁₄H₁₅BN₂
• Molecular Weight: 222.097
• Mol file: 1365973-61-0.mol

Synonyms:

Chemical Property of HB(N,N'-diphenyl-1,2-ethylenediamine(-2H))

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of HB(N,N'-diphenyl-1,2-ethylenediamine(-2H))

There total 2 articles about HB(N,N'-diphenyl-1,2-ethylenediamine(-2H)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N'-diphenylethylenediamine (150-61-8) → HB(N,N'-diphenyl-1,2-ethylenediamine(-2H)) (1365973-61-0)

Guidance literature:

With borane-THF; In tetrahydrofuran;

DOI:10.1021/ja210542r

Reference yield:

borane-THF (14044-65-6) + N,N'-diphenylethylenediamine (150-61-8) → HB(N,N'-diphenyl-1,2-ethylenediamine(-2H)) (1365973-61-0) + N,N'-diphenyl-1,2-ethylenediamine-borane (1/2)

Guidance literature:

In tetrahydrofuran; 1,2-dimethoxyethane; (inert atm.); addn. of THF soln. of borane to DME soln. of diamine deriv., keeping at 20°C for 6 h; NMR;

DOI:10.1021/ja210542r

upstream raw materials:

borane-THF

N,N'-diphenylethylenediamine