C₃₁H₃₆N₂O₄

Base Information

Chemical Name:C₃₁H₃₆N₂O₄
CAS No.:1609200-15-8
Molecular Formula:C₃₁H₃₆N₂O₄
Molecular Weight:500.638
Hs Code.:

C<sub>31</sub>H<sub>36</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:

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Chemical Property of C₃₁H₃₆N₂O₄

Chemical Property:

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Technology Process of C₃₁H₃₆N₂O₄

There total 9 articles about C₃₁H₃₆N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1318759-39-5
2-(2-(tetrahydro-2H-pyran-2-yloxy)ethyl)-1H-indole

: 1609200-15-8
C₃₁H₃₆N₂O₄

Guidance literature:: Multi-step reaction with 10 steps

1: triethylamine; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

2: toluene-4-sulfonic acid / methanol / 14 h / 20 °C / Inert atmosphere

3: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

4: potassium carbonate / N,N-dimethyl-formamide / 3 h / 50 °C / Inert atmosphere

5: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol / tert-butyl methyl ether; hexane / 6 h / 40 °C

6: potassium hydroxide / methanol / 3.5 h / Inert atmosphere; Reflux

7: trichlorophosphate / toluene / 0.5 h / Inert atmosphere; Reflux

8: sodium tetrahydroborate / methanol / 3 h / 0 °C / Inert atmosphere

9: triethylamine; dmap / dichloromethane / 12 h / 20 °C / Inert atmosphere

10: sodium carbonate / dichloromethane / 12 h / 20 °C / Inert atmosphere

With 1H-imidazole; dmap; sodium tetrahydroborate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; iodine; sodium carbonate; potassium carbonate; toluene-4-sulfonic acid; triethylamine; triphenylphosphine; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol; potassium hydroxide; trichlorophosphate; In methanol; hexane; dichloromethane; tert-butyl methyl ether; N,N-dimethyl-formamide; toluene; 7: |Bischler-Napieralski Reaction;
DOI:10.1039/c4cc01843e

Reference yield:

: C₂₀H₂₇NO₄

: 1609200-15-8
C₃₁H₃₆N₂O₄

Guidance literature:: Multi-step reaction with 9 steps

1: toluene-4-sulfonic acid / methanol / 14 h / 20 °C / Inert atmosphere

2: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

3: potassium carbonate / N,N-dimethyl-formamide / 3 h / 50 °C / Inert atmosphere

4: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol / tert-butyl methyl ether; hexane / 6 h / 40 °C

5: potassium hydroxide / methanol / 3.5 h / Inert atmosphere; Reflux

6: trichlorophosphate / toluene / 0.5 h / Inert atmosphere; Reflux

7: sodium tetrahydroborate / methanol / 3 h / 0 °C / Inert atmosphere

8: triethylamine; dmap / dichloromethane / 12 h / 20 °C / Inert atmosphere

9: sodium carbonate / dichloromethane / 12 h / 20 °C / Inert atmosphere

With 1H-imidazole; dmap; sodium tetrahydroborate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; iodine; sodium carbonate; potassium carbonate; toluene-4-sulfonic acid; triethylamine; triphenylphosphine; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol; potassium hydroxide; trichlorophosphate; In methanol; hexane; dichloromethane; tert-butyl methyl ether; N,N-dimethyl-formamide; toluene; 6: |Bischler-Napieralski Reaction;
DOI:10.1039/c4cc01843e

Reference yield:

: 1334651-33-0
tert-butyl 2-(2-hydroxyethyl)-1H-indole-1-carboxylate

: 1609200-15-8
C₃₁H₃₆N₂O₄

Guidance literature:: Multi-step reaction with 8 steps

1: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 3 h / 50 °C / Inert atmosphere

3: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol / tert-butyl methyl ether; hexane / 6 h / 40 °C

4: potassium hydroxide / methanol / 3.5 h / Inert atmosphere; Reflux

5: trichlorophosphate / toluene / 0.5 h / Inert atmosphere; Reflux

6: sodium tetrahydroborate / methanol / 3 h / 0 °C / Inert atmosphere

7: triethylamine; dmap / dichloromethane / 12 h / 20 °C / Inert atmosphere

8: sodium carbonate / dichloromethane / 12 h / 20 °C / Inert atmosphere

With 1H-imidazole; dmap; sodium tetrahydroborate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; iodine; sodium carbonate; potassium carbonate; triethylamine; triphenylphosphine; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol; potassium hydroxide; trichlorophosphate; In methanol; hexane; dichloromethane; tert-butyl methyl ether; N,N-dimethyl-formamide; toluene; 5: |Bischler-Napieralski Reaction;
DOI:10.1039/c4cc01843e