sodium rac-1-[3,5-bis(trifluoromethyl)phenyl]ethyl sulfate

Base Information

Chemical Name:sodium rac-1-[3,5-bis(trifluoromethyl)phenyl]ethyl sulfate
CAS No.:1384108-58-0
Molecular Formula:C₁₀H₇F₆O₄S*Na
Molecular Weight:360.209
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of sodium rac-1-[3,5-bis(trifluoromethyl)phenyl]ethyl sulfate

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Technology Process of sodium rac-1-[3,5-bis(trifluoromethyl)phenyl]ethyl sulfate

There total 1 articles about sodium rac-1-[3,5-bis(trifluoromethyl)phenyl]ethyl sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68120-60-5,127852-28-2,368-63-8
1-(3,5-bis(trifluoromethyl)phenyl)ethan-1-ol

: 1384108-58-0
sodium rac-1-[3,5-bis(trifluoromethyl)phenyl]ethyl sulfate

Guidance literature:: With triethylamine sulfur trioxide; sodium hydride; In paraffin oil;
DOI:10.1002/adsc.201100864

Reference yield:

: 1384108-58-0
sodium rac-1-[3,5-bis(trifluoromethyl)phenyl]ethyl sulfate

: 1384108-70-6
sodium (S)-1-[3,5-bis(trifluoromethyl)phenyl]ethyl sulfate

: 225920-05-8
(S)-3,5-bis(trifluoromethyl)-1-phenylethanol

Guidance literature:: With PISA₁ sulfatase; water; In aq. buffer; for 72h; pH=8; enantioselective reaction; Enzymatic reaction;
DOI:10.1002/anie.201209946

Reference yield:

: 1384108-58-0
sodium rac-1-[3,5-bis(trifluoromethyl)phenyl]ethyl sulfate

: 225920-05-8
(S)-3,5-bis(trifluoromethyl)-1-phenylethanol

Guidance literature:: Multi-step reaction with 2 steps

1: sec-alkylsulfatase Pisa₁ / dimethyl sulfoxide / 72 h / 30 °C / pH 8.2 / aq. buffer; Enzymatic reaction

2: toluene-4-sulfonic acid / 1,4-dioxane; tert-butyl methyl ether; water / 2 h / 40 °C

With sec-alkylsulfatase Pisa₁; toluene-4-sulfonic acid; In 1,4-dioxane; tert-butyl methyl ether; water; dimethyl sulfoxide;
DOI:10.1002/adsc.201100864