C₂₉H₃₀O₇

Base Information

Chemical Name:C₂₉H₃₀O₇
CAS No.:1443651-26-0
Molecular Formula:C₂₉H₃₀O₇
Molecular Weight:490.553
Hs Code.:

C<sub>29</sub>H<sub>30</sub>O<sub>7</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₃₀O₇

Chemical Property:

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Technology Process of C₂₉H₃₀O₇

There total 18 articles about C₂₉H₃₀O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₃₂O₈

: 1443651-26-0
C₂₉H₃₀O₇

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/chem.201204545

Reference yield:

: 1443651-22-6
C₁₉H₂₂O₆

: 1443651-26-0
C₂₉H₃₀O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium hydrochloride monohydrate / tetrahydrofuran; water / 18 h / 20 °C

2.1: 12 h / 0 - 20 °C / Inert atmosphere

2.2: 3 h / 0 - 20 °C / Inert atmosphere

3.1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine / tetrahydrofuran; cyclohexane / 0.25 h / 20 °C / Inert atmosphere

3.2: 48 h / 85 °C / Inert atmosphere

4.1: tetrahydrofuran; water / 7 h / 20 °C

5.1: chloro-trimethyl-silane / tetrahydrofuran; water / 0.33 h / 20 °C

5.2: 4 h / 70 °C

6.1: lithium hydrochloride monohydrate / tetrahydrofuran; water / 18 h / 20 °C

7.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

With dmap; chloro-trimethyl-silane; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; lithium hydrochloride monohydrate; dicyclohexyl-carbodiimide; 4,4'-di-tert-butyl-2,2'-bipyridine; In tetrahydrofuran; dichloromethane; cyclohexane; water; 5.2: |Suzuki Coupling;
DOI:10.1002/chem.201204545

Reference yield:

: 1443651-21-5
C₂₃H₃₀O₆

: 1443651-26-0
C₂₉H₃₀O₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: boron tribromide / dichloromethane / 12 h / -78 - 20 °C / Inert atmosphere

2.1: lithium hydrochloride monohydrate / tetrahydrofuran; water / 18 h / 20 °C

3.1: 12 h / 0 - 20 °C / Inert atmosphere

3.2: 3 h / 0 - 20 °C / Inert atmosphere

4.1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine / tetrahydrofuran; cyclohexane / 0.25 h / 20 °C / Inert atmosphere

4.2: 48 h / 85 °C / Inert atmosphere

5.1: tetrahydrofuran; water / 7 h / 20 °C

6.1: chloro-trimethyl-silane / tetrahydrofuran; water / 0.33 h / 20 °C

6.2: 4 h / 70 °C

7.1: lithium hydrochloride monohydrate / tetrahydrofuran; water / 18 h / 20 °C

8.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

With dmap; chloro-trimethyl-silane; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; lithium hydrochloride monohydrate; boron tribromide; dicyclohexyl-carbodiimide; 4,4'-di-tert-butyl-2,2'-bipyridine; In tetrahydrofuran; dichloromethane; cyclohexane; water; 6.2: |Suzuki Coupling;
DOI:10.1002/chem.201204545