Technology Process of C18H27BrO4
There total 6 articles about C18H27BrO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
In
ethanol;
at 0 ℃;
DOI:10.1021/ja4018122
- Guidance literature:
-
Multi-step reaction with 5 steps
1: magnesium chloride; triethylamine / tetrahydrofuran / 20 °C
2: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C
3: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C
4: copper dichloride; water / acetonitrile / Reflux
5: sodium tetrahydroborate / ethanol / 0 °C
With
sodium tetrahydroborate; di-isopropyl azodicarboxylate; potassium tert-butylate; water; triethylamine; triphenylphosphine; copper dichloride; magnesium chloride;
In
tetrahydrofuran; ethanol; acetonitrile;
DOI:10.1021/ja4018122
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C
2: copper dichloride; water / acetonitrile / Reflux
3: sodium tetrahydroborate / ethanol / 0 °C
With
sodium tetrahydroborate; di-isopropyl azodicarboxylate; water; triphenylphosphine; copper dichloride;
In
tetrahydrofuran; ethanol; acetonitrile;
DOI:10.1021/ja4018122