Technology Process of 3,9-epoxy-p-menthyl-10-tosylate
There total 6 articles about 3,9-epoxy-p-menthyl-10-tosylate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 76 percent / meta-chloroperbenzoic acid / CH2Cl2 / 2 h / Ambient temperature
2: 64 percent / lithium diisopropylamide / diethyl ether / 6 h / Ambient temperature
3: 1.) B2H6, 2.) H2O2, aq. NaOH / 1) THF, 25 deg C, 3 h; 2) 30 - 40 deg C, 1 h
4: 53 percent / lead tetraacetate, calcium carbonate / benzene / 2 h / Heating
5: pyridine / 24 h / Ambient temperature
With
pyridine; lead(IV) acetate; sodium hydroxide; dihydrogen peroxide; 3-chloro-benzenecarboperoxoic acid; calcium carbonate; diborane; lithium diisopropyl amide;
In
diethyl ether; dichloromethane; benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) B2H6, 2.) H2O2, aq. NaOH / 1) THF, 25 deg C, 3 h; 2) 30 - 40 deg C, 1 h
2: 53 percent / lead tetraacetate, calcium carbonate / benzene / 2 h / Heating
3: pyridine / 24 h / Ambient temperature
With
pyridine; lead(IV) acetate; sodium hydroxide; dihydrogen peroxide; calcium carbonate; diborane;
In
benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 64 percent / lithium diisopropylamide / diethyl ether / 6 h / Ambient temperature
2: 1.) B2H6, 2.) H2O2, aq. NaOH / 1) THF, 25 deg C, 3 h; 2) 30 - 40 deg C, 1 h
3: 53 percent / lead tetraacetate, calcium carbonate / benzene / 2 h / Heating
4: pyridine / 24 h / Ambient temperature
With
pyridine; lead(IV) acetate; sodium hydroxide; dihydrogen peroxide; calcium carbonate; diborane; lithium diisopropyl amide;
In
diethyl ether; benzene;