C₂₅H₄₂O₄Si

Base Information Edit

Chemical Name:C₂₅H₄₂O₄Si
CAS No.:105880-45-3
Molecular Formula:C₂₅H₄₂O₄Si
Molecular Weight:434.692
Hs Code.:
Mol file:105880-45-3.mol

C<sub>25</sub>H<sub>42</sub>O<sub>4</sub>Si

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Chemical Property of C₂₅H₄₂O₄Si Edit

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Technology Process of C₂₅H₄₂O₄Si

There total 9 articles about C₂₅H₄₂O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 97563-45-6,105880-38-4,128241-52-1,4187-88-6
1-cyclohexylprop-2-yn-1-ol

: 105880-45-3
C₂₅H₄₂O₄Si

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / chromium trioxide, conc. sulfuric acid / acetone / 1 h / 0 °C

2: 1.) (S)-Alpine Borane, 2.) sodium hydroxide, 30 percent hydrogen peroxide / 1.) THF, 23 deg C, 16 h, 2.) THF, 40 deg C, 3 h

3: 71 percent / triethylamine / CH₂Cl₂ / 15 h / Ambient temperature

4: 1.) n-butyllithium, 2.) boron trifluoride etherate / 1.) THF, hexane, 2.) THF, hexane, -78 deg C

With chromium(VI) oxide; sodium hydroxide; n-butyllithium; (S)-alpine borane; sulfuric acid; boron trifluoride diethyl etherate; dihydrogen peroxide; triethylamine; In dichloromethane; acetone;
DOI:10.1021/jo00389a038

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 105880-45-3
C₂₅H₄₂O₄Si

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) ethylmagnesium bromide / 1.) THF, 2.) THF, 23 deg C, 16 h

2: 82 percent / chromium trioxide, conc. sulfuric acid / acetone / 1 h / 0 °C

3: 1.) (S)-Alpine Borane, 2.) sodium hydroxide, 30 percent hydrogen peroxide / 1.) THF, 23 deg C, 16 h, 2.) THF, 40 deg C, 3 h

4: 71 percent / triethylamine / CH₂Cl₂ / 15 h / Ambient temperature

5: 1.) n-butyllithium, 2.) boron trifluoride etherate / 1.) THF, hexane, 2.) THF, hexane, -78 deg C

With chromium(VI) oxide; sodium hydroxide; n-butyllithium; (S)-alpine borane; sulfuric acid; boron trifluoride diethyl etherate; ethylmagnesium bromide; dihydrogen peroxide; triethylamine; In dichloromethane; acetone;
DOI:10.1021/jo00389a038

Reference yield:

: 7560-69-2
1-cyclohexyl-2-propyn-1-one

: 105880-45-3
C₂₅H₄₂O₄Si

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) (S)-Alpine Borane, 2.) sodium hydroxide, 30 percent hydrogen peroxide / 1.) THF, 23 deg C, 16 h, 2.) THF, 40 deg C, 3 h

2: 71 percent / triethylamine / CH₂Cl₂ / 15 h / Ambient temperature

3: 1.) n-butyllithium, 2.) boron trifluoride etherate / 1.) THF, hexane, 2.) THF, hexane, -78 deg C

With sodium hydroxide; n-butyllithium; (S)-alpine borane; boron trifluoride diethyl etherate; dihydrogen peroxide; triethylamine; In dichloromethane;
DOI:10.1021/jo00389a038