(OC)₃Fe((CH₂)₃S₂)Ni(Ph₂P(CH₂)₂PPh₂)

Base Information

Chemical Name:(OC)₃Fe((CH₂)₃S₂)Ni(Ph₂P(CH₂)₂PPh₂)
CAS No.:877034-22-5
Molecular Formula:C₃₂H₃₀FeNiO₃P₂S₂
Molecular Weight:703.205
Hs Code.:

(OC)<SUB>3</SUB>Fe((CH<SUB>2</SUB>)<SUB>3</SUB>S<SUB>2</SUB>)Ni(Ph<SUB>2</SUB>P(CH<SUB>2</SUB>)<SUB>2</SUB>PPh<SUB>2</SUB>)

Synonyms:

Suppliers and Price of (OC)₃Fe((CH₂)₃S₂)Ni(Ph₂P(CH₂)₂PPh₂)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (OC)₃Fe((CH₂)₃S₂)Ni(Ph₂P(CH₂)₂PPh₂)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (OC)₃Fe((CH₂)₃S₂)Ni(Ph₂P(CH₂)₂PPh₂)

There total 7 articles about (OC)₃Fe((CH₂)₃S₂)Ni(Ph₂P(CH₂)₂PPh₂) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 15616-56-5,14911-55-8,14878-30-9
diiodotetracarbonyliron(II)

: 61703-81-9
[nickel(II)(1,3-propanedithiolate)(1,2-bis(diphenylphosphino)ethane)]

: 877034-21-4,877034-22-5
(OC)₃Fe((CH₂)₃S₂)Ni(Ph₂P(CH₂)₂PPh₂)

Guidance literature:: With (C₅H₅)2Co; In dichloromethane; using Schlenk techniques; CH2Cl2 added to mixt. of Fe complex and Ni complex at -78°C; treated with (C5H5)2Co; stirred at room temp. for 1 h; evapd. under reduced pressure; washed and sonicated with MeCN; extd. into CH2Cl2; filtered through Celite; filtrate concd. to dryness under vac.;
DOI:10.1021/ic2012759

Reference yield: 27.0%

: 15321-51-4
diiron nonacarbonyl

: 61703-81-9
[nickel(II)(1,3-propanedithiolate)(1,2-bis(diphenylphosphino)ethane)]

: 13463-40-6,37220-42-1
iron pentacarbonyl

: 1,3-(μ-propanedithiolato)diironhexacarbonyl

: 877034-21-4,877034-22-5
(OC)₃Fe((CH₂)₃S₂)Ni(Ph₂P(CH₂)₂PPh₂)

Guidance literature:: In dichloromethane; (Schlenk) a soln. of Fe-complex and Ni-complex in CH2Cl2 was stirred for6 h; the solvent was removed under vac., the residue was washed with CH3CN, extd. with CH2Cl2, filtered through silica gel, rinsed with CH2Cl2, concd., diluted with hexane;
DOI:10.1021/ja105312p