Methyl Cyclohexylidenephenoxyacetate

Base Information

Chemical Name:Methyl Cyclohexylidenephenoxyacetate
CAS No.:69515-13-5
Molecular Formula:C₁₅H₁₈O₃
Molecular Weight:246.306
Hs Code.:

Synonyms:

Suppliers and Price of Methyl Cyclohexylidenephenoxyacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl Cyclohexylidenephenoxyacetate

Chemical Property:

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Technology Process of Methyl Cyclohexylidenephenoxyacetate

There total 3 articles about Methyl Cyclohexylidenephenoxyacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2065-23-8
methyl 2-phenoxyacetate

: 69515-13-5
Methyl Cyclohexylidenephenoxyacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / N-bromosuccinimide / benzene / 0.5 h / Irradiation

2: 89 percent / 1.) steam bath, 12 min.; 2.) room temp. overnight

3: 1.) NaH / 1.) DME, 70 deg C, 45 min.; 2.) reflux, 6h

With N-Bromosuccinimide; sodium hydride; In benzene;
DOI:10.1021/jo00168a008

Reference yield:

: 86728-16-7
methyl α-bromo-2-phenoxyacetate

: 69515-13-5
Methyl Cyclohexylidenephenoxyacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / 1.) steam bath, 12 min.; 2.) room temp. overnight

2: 1.) NaH / 1.) DME, 70 deg C, 45 min.; 2.) reflux, 6h

With sodium hydride;
DOI:10.1021/jo00168a008

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 86728-17-8
methyl 2-phenoxy-2-diethylphosphonoacetate

: 69515-13-5
Methyl Cyclohexylidenephenoxyacetate

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DME, 70 deg C, 45 min.; 2.) reflux, 6h;
DOI:10.1021/jo00168a008