Technology Process of C11H17NO
There total 4 articles about C11H17NO which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: acetic anhydride / 1 h / 20 °C
1.2: 0.17 h / 20 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Cooling with ice; Reflux
With
lithium aluminium tetrahydride; acetic anhydride;
In
tetrahydrofuran;
DOI:10.1021/ja206744z
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tris-(dibenzylideneacetone)dipalladium(0); potassium hydroxide; tert-butyl XPhos / 1,4-dioxane / 24 h / 90 °C / Inert atmosphere
2.1: hydrogen / methanol / 14 h / 20 °C
3.1: acetic anhydride / 1 h / 20 °C
3.2: 0.17 h / 20 °C
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Cooling with ice; Reflux
With
tris-(dibenzylideneacetone)dipalladium(0); lithium aluminium tetrahydride; hydrogen; acetic anhydride; potassium hydroxide; tert-butyl XPhos;
In
tetrahydrofuran; 1,4-dioxane; methanol;
DOI:10.1021/ja206744z
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogen / methanol / 14 h / 20 °C
2.1: acetic anhydride / 1 h / 20 °C
2.2: 0.17 h / 20 °C
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Cooling with ice; Reflux
With
lithium aluminium tetrahydride; hydrogen; acetic anhydride;
In
tetrahydrofuran; methanol;
DOI:10.1021/ja206744z
