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InH3(C3H2N2(C9H11)2)

Base Information
  • Chemical Name:InH3(C3H2N2(C9H11)2)
  • CAS No.:311311-56-5
  • Molecular Formula:C21H27InN2
  • Molecular Weight:422.279
  • Hs Code.:
InH<sub>3</sub>(C<sub>3</sub>H<sub>2</sub>N<sub>2</sub>(C<sub>9</sub>H<sub>11</sub>)2)

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Chemical Property of InH3(C3H2N2(C9H11)2)
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Technology Process of InH3(C3H2N2(C9H11)2)

There total 3 articles about InH3(C3H2N2(C9H11)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In water; ethylene glycol; other Radiation; Ir complex and ligand suspended in ethylene glycol, under purging N2 atm. suspn. subjected to reflux for 15 min in microwawe oven with frequencyof 2450 MHz, cooled to room temp., pptd. with satd. aq. soln. of KPF6; filtered, recrystd. from MeCN/Et2O;
DOI:10.1246/cl.2000.1206
Guidance literature:
In diethyl ether; stirred for 2 h at room temp.; solvent removed in vacuo, residue dissolved in toluene, filtd., storage for 24 h at -35°C, crystals sepd.; elem. anal.;
DOI:10.1021/om0004951
Guidance literature:
In diethyl ether; stirred for 2.5 h at -50°C, added C3H2N2(C9H11)2 and stirred for 2 h at -20°C; ppt. collected and recrystd. from toluene at -35°C;
DOI:10.1021/om0004951
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