(S)-(+)-methyl 3-<4-<2-ethoxy>phenyl>-2-acetoxypropanoate

Base Information

Chemical Name:(S)-(+)-methyl 3-<4-<2-ethoxy>phenyl>-2-acetoxypropanoate
CAS No.:239478-57-0
Molecular Formula:C₂₂H₂₄N₂O₆
Molecular Weight:412.442
Hs Code.:

(S)-(+)-methyl 3-<4-<2-<N-(2-benzoxazolyl)-N-methylamino>ethoxy>phenyl>-2-acetoxypropanoate

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Chemical Property of (S)-(+)-methyl 3-<4-<2-ethoxy>phenyl>-2-acetoxypropanoate

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Technology Process of (S)-(+)-methyl 3-<4-<2-ethoxy>phenyl>-2-acetoxypropanoate

There total 4 articles about (S)-(+)-methyl 3-<4-<2-ethoxy>phenyl>-2-acetoxypropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 108-05-4,9003-20-7
vinyl acetate

: 158062-59-0
methyl 3-<4-<2-ethoxy>phenyl>-2-hydroxypropanoate

: 239478-56-9
(R)-(+)-methyl 3-<4-<2-ethoxy>phenyl>-2-hydroxypropanoate

: 239478-57-0
(S)-(+)-methyl 3-<4-<2-ethoxy>phenyl>-2-acetoxypropanoate

Guidance literature:: With pseudomonas fluorescens lipase; for 144h; Ambient temperature;
DOI:10.1016/S0968-0896(99)00034-6

Reference yield:

: 128316-64-3,481072-37-1
(+/-)-methyl 3-p-benzyloxyphenyl-2-hydroxypropionate

: 239478-57-0
(S)-(+)-methyl 3-<4-<2-ethoxy>phenyl>-2-acetoxypropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / H₂ / Pd/C / methanol / Ambient temperature

2: 37 percent / NaH / dimethylformamide / 16 h / 80 °C

3: 43 percent / Pseudomonas Fluorescens lipase / 144 h / Ambient temperature

With pseudomonas fluorescens lipase; hydrogen; sodium hydride; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(99)00034-6

Reference yield:

: 51095-47-7
methyl 3-(4-hydroxyphenyl)-2-hydroxypropionate

: 239478-57-0
(S)-(+)-methyl 3-<4-<2-ethoxy>phenyl>-2-acetoxypropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 37 percent / NaH / dimethylformamide / 16 h / 80 °C

2: 43 percent / Pseudomonas Fluorescens lipase / 144 h / Ambient temperature

With pseudomonas fluorescens lipase; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(99)00034-6