6''-O-<2-(methoxycarbonyl)acetyl>isoquercitrin

Base Information

Chemical Name:6''-O-<2-(methoxycarbonyl)acetyl>isoquercitrin
CAS No.:153874-66-9
Molecular Formula:C₂₅H₂₄O₁₅
Molecular Weight:564.457
Hs Code.:

Synonyms:

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Chemical Property of 6''-O-<2-(methoxycarbonyl)acetyl>isoquercitrin

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Technology Process of 6''-O-<2-(methoxycarbonyl)acetyl>isoquercitrin

There total 1 articles about 6''-O-<2-(methoxycarbonyl)acetyl>isoquercitrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 482-35-9
isoquercetin

: 131072-45-2
2-chloroethyl methyl propanedioate

: 3''-O-<2-(methoxycarbonyl)acetyl>isoquercitrin

: 153874-66-9
6''-O-<2-(methoxycarbonyl)acetyl>isoquercitrin

: 3'',6''-di-O-<2-(methoxycarbonyl)acetyl>isoquercitrin

Guidance literature:: In pyridine; at 45 ℃; for 168h; subtilisin;
DOI:10.1002/hlca.19930760823

Reference yield: 33.0%

: 153874-66-9
6''-O-<2-(methoxycarbonyl)acetyl>isoquercitrin

: 482-35-9
isoquercetin

: 96862-01-0
quercetin 3-O-(6′′-O-malonyl)-β-glucopyranoside

Guidance literature:: With phosphate buffer pH 7; pig-liver esterase; In N,N-dimethyl-formamide; for 24h; Product distribution; Ambient temperature; various enzymes;
DOI:10.1002/hlca.19930760823

Reference yield:

: 153874-66-9
6''-O-<2-(methoxycarbonyl)acetyl>isoquercitrin

: ((2R,3S,4S,5R,6S)-6-((2-(3,4-dihydroxyphenyl)-5,7-dihydroxy-4-oxo-4H-chromen-3-yl)oxy)-3,4,5-trihydroxytetrahydro-2H-pyran-2-yl)methyl cinnamate

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / pig-liver esterase, phosphate buffer pH 7 / dimethylformamide / 24 h / Ambient temperature; various enzymes

2: 32 mg / piperidine, molecular sieves / pyridine / 2.5 h / 60 °C

With piperidine; molecular sieve; phosphate buffer pH 7; pig-liver esterase; In pyridine; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19930760823