C₆H₇ClN₂O₂

Base Information

• Chemical Name: C₆H₇ClN₂O₂
• CAS No.: 1354455-01-8
• Molecular Formula: C₆H₇ClN₂O₂
• Molecular Weight: 174.587

Synonyms:

Chemical Property of C₆H₇ClN₂O₂

Chemical Property:

• Density: 1.53±0.1 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

5-Chloro-4-(2-hydroxyethyl)pyridazin-3-ol 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆H₇ClN₂O₂

There total 3 articles about C₆H₇ClN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

C14H15ClN2O3 → C6H7ClN2O2 (1354455-01-8)

Guidance literature:

With ammonium cerium (IV) nitrate; water; In acetonitrile; at 0 - 23 ℃;

DOI:10.1016/j.tetlet.2011.11.070

Reference yield:

2-[5-chloro-2-(4-methoxybenzyl)-3-oxo-2,3-dihydro-pyridazine-4-yl]-malonic acid diethyl ester (1037507-98-4) → C6H7ClN2O2 (1354455-01-8)

Guidance literature:

Multi-step reaction with 3 steps

1: water / dimethyl sulfoxide / 135 °C

2: sodium tetrahydroborate / ethanol / 0 - 23 °C

3: ammonium cerium (IV) nitrate; water / acetonitrile / 0 - 23 °C

With sodium tetrahydroborate; ammonium cerium (IV) nitrate; water; In ethanol; dimethyl sulfoxide; acetonitrile;

DOI:10.1016/j.tetlet.2011.11.070

Reference yield:

[5-chloro-2-(4-methoxybenzyl)-3-oxo-2,3-dihydro-pyridazine-4-yl]-acetic acid ethyl ester (1037508-01-2) → C6H7ClN2O2 (1354455-01-8)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / 0 - 23 °C

2: ammonium cerium (IV) nitrate; water / acetonitrile / 0 - 23 °C

With sodium tetrahydroborate; ammonium cerium (IV) nitrate; water; In ethanol; acetonitrile;

DOI:10.1016/j.tetlet.2011.11.070

upstream raw materials:

2-[5-chloro-2-(4-methoxybenzyl)-3-oxo-2,3-dihydro-pyridazine-4-yl]-malonic acid diethyl ester

[5-chloro-2-(4-methoxybenzyl)-3-oxo-2,3-dihydro-pyridazine-4-yl]-acetic acid ethyl ester

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