triphenylphosphine-ethoxycarbonylborane

Base Information

• Chemical Name: triphenylphosphine-ethoxycarbonylborane
• CAS No.: 78315-29-4
• Molecular Formula: C₂₁H₂₂BO₂P
• Molecular Weight: 348.189
• Mol file: 78315-29-4.mol

Synonyms:

Chemical Property of triphenylphosphine-ethoxycarbonylborane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of triphenylphosphine-ethoxycarbonylborane

There total 1 articles about triphenylphosphine-ethoxycarbonylborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

triphenylphosphine-cyanoborane (67374-60-1) → triphenylphosphine-ethoxycarbonylborane (78315-29-4)

Guidance literature:

With ethanol; triethyloxonium fluoroborate; hydrogen cation; In dichloromethane; soln. of the B-compd. and Et3OBF4 in CH2Cl2 refluxed for 20 h, cooled, CH2Cl2 removed at reduced pressure, treated with H2O, stirred for 44 h, extd. with CH2Cl2, combined extracts dried over MgSO4, filtered, solventremoved, dissolved in hot EtOH; pptd. with cooling and addn. of H2O, elem. anal.;

DOI:10.1016/0022-1902(81)80483-6

upstream raw materials:

triphenylphosphine-cyanoborane