Technology Process of C32H43N3O8
There total 10 articles about C32H43N3O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium nitrososulfonate;
In
ethyl acetate;
at 20 ℃;
for 0.75h;
aq. phosphate buffer;
DOI:10.1002/chem.201103605
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: sodium hydroxide / water
1.3: 215 °C
2.1: trichlorophosphate / N,N-dimethyl-formamide
3.1: ammonium acetate
4.1: lithium aluminium tetrahydride
5.1: dmap
6.1: tetrakis(triphenylphosphine) palladium(0); copper(l) chloride; lithium chloride
7.1: ammonium acetate; palladium
8.1: potassium nitrososulfonate / ethyl acetate / 0.75 h / 20 °C / aq. phosphate buffer
With
dmap; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium(0); potassium nitrososulfonate; ammonium acetate; palladium; copper(l) chloride; lithium chloride; sodium hydroxide; trichlorophosphate;
In
water; ethyl acetate; N,N-dimethyl-formamide;
3.1: Henry reaction;
DOI:10.1002/chem.201103605
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap
2: tetrakis(triphenylphosphine) palladium(0); copper(l) chloride; lithium chloride
3: ammonium acetate; palladium
4: potassium nitrososulfonate / ethyl acetate / 0.75 h / 20 °C / aq. phosphate buffer
With
dmap; tetrakis(triphenylphosphine) palladium(0); potassium nitrososulfonate; ammonium acetate; palladium; copper(l) chloride; lithium chloride;
In
ethyl acetate;
DOI:10.1002/chem.201103605
