O-d4-2-iodobenzoyl-N,N-d10-dibenzylhydroxylamine

Base Information

Chemical Name:O-d4-2-iodobenzoyl-N,N-d10-dibenzylhydroxylamine
CAS No.:936138-64-6
Molecular Formula:C₂₁H₁₈INO₂
Molecular Weight:457.173
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-d4-2-iodobenzoyl-N,N-d10-dibenzylhydroxylamine

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Technology Process of O-d4-2-iodobenzoyl-N,N-d10-dibenzylhydroxylamine

There total 6 articles about O-d4-2-iodobenzoyl-N,N-d10-dibenzylhydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 923282-09-1
N,N-bis[2,3,4,5,6-2H₅]benzylamine

: 936138-64-6
O-d4-2-iodobenzoyl-N,N-d10-dibenzylhydroxylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 48 percent / potassium hydrogen phosphate / diethyl ether / 72 h / Heating

2: 66 percent / potassium methoxide / methanol; diethyl ether / 36 h / 20 °C

3: 100 percent / 4-(dimethylamino)pyridine; dicyclohexylcarbodiimide / CH₂Cl₂ / 0.83 h

With dmap; dipotassium hydrogenphosphate; potassium methanolate; dicyclohexyl-carbodiimide; In methanol; diethyl ether; dichloromethane;
DOI:10.1021/ol0702829

Reference yield:

: 936138-60-2
ethyl d4-2-iodobenzoate

: 936138-64-6
O-d4-2-iodobenzoyl-N,N-d10-dibenzylhydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / potassium hydroxide / methanol / 16 h / 20 °C

2: 100 percent / 4-(dimethylamino)pyridine; dicyclohexylcarbodiimide / CH₂Cl₂ / 0.83 h

With dmap; potassium hydroxide; dicyclohexyl-carbodiimide; In methanol; dichloromethane;
DOI:10.1021/ol0702829

Reference yield:

: 936138-62-4
O-benzoyl-N,N-d10-dibenzylamine

: 936138-64-6
O-d4-2-iodobenzoyl-N,N-d10-dibenzylhydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / potassium methoxide / methanol; diethyl ether / 36 h / 20 °C

2: 100 percent / 4-(dimethylamino)pyridine; dicyclohexylcarbodiimide / CH₂Cl₂ / 0.83 h

With dmap; potassium methanolate; dicyclohexyl-carbodiimide; In methanol; diethyl ether; dichloromethane;
DOI:10.1021/ol0702829