1-bromoethyl p-tolyl sulfoxide

Base Information

Chemical Name:1-bromoethyl p-tolyl sulfoxide
CAS No.:31350-97-7
Molecular Formula:C₉H₁₁BrOS
Molecular Weight:247.156
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-bromoethyl p-tolyl sulfoxide

Chemical Property:

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Technology Process of 1-bromoethyl p-tolyl sulfoxide

There total 1 articles about 1-bromoethyl p-tolyl sulfoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 6378-07-0
ethyl (p-tolyl)sulfoxide

: 31350-97-7
1-bromoethyl p-tolyl sulfoxide

Guidance literature:: With N-Bromosuccinimide; silica gel; for 36h; Ambient temperature;
DOI:10.1055/s-1986-31793

Reference yield:

: 31350-97-7
1-bromoethyl p-tolyl sulfoxide

: 141054-32-2
1-Phenyl-4-(toluene-4-sulfonyl)-pentan-3-one

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) LDA / 1.) THF, -60 deg C, 2.) THF

2: 3-chloroperoxybenzoic acid / CH₂Cl₂ / Ambient temperature

3: 100 percent / Swern oxidation reagent

4: 1.) n-BuLi / 1.) THF, -60 deg C, 2.) THF

With n-butyllithium; Swern oxidation reagent; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In dichloromethane;
DOI:10.1246/cl.1992.381

Reference yield:

: 31350-97-7
1-bromoethyl p-tolyl sulfoxide

: 4-Bromo-1-phenyl-4-(toluene-4-sulfonyl)-pentan-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA / 1.) THF, -60 deg C, 2.) THF

2: 3-chloroperoxybenzoic acid / CH₂Cl₂ / Ambient temperature

3: 100 percent / Swern oxidation reagent

With Swern oxidation reagent; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In dichloromethane;
DOI:10.1246/cl.1992.381