diphenyl-1,3 diacetoxy-4,7 benzothiophene

Base Information

Chemical Name:diphenyl-1,3 diacetoxy-4,7 benzothiophene
CAS No.:127441-66-1
Molecular Formula:C₂₄H₁₈O₄S
Molecular Weight:402.471
Hs Code.:

diphenyl-1,3 diacetoxy-4,7 benzo<c>thiophene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphenyl-1,3 diacetoxy-4,7 benzothiophene

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Technology Process of diphenyl-1,3 diacetoxy-4,7 benzothiophene

There total 2 articles about diphenyl-1,3 diacetoxy-4,7 benzothiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 68145-15-3
diphenyl-1,3 benzothiophenedione-4,7

: 108-24-7
acetic anhydride

: 127441-66-1
diphenyl-1,3 diacetoxy-4,7 benzothiophene

Guidance literature:: With pyridine; zinc; for 0.0333333h; Heating;

Reference yield:

: 74962-83-7
diphenyldimethoxybenzothiophene

: 127441-66-1
diphenyl-1,3 diacetoxy-4,7 benzothiophene

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / cerium ammonium nitrate / acetonitrile; H₂O / 0.5 h / Ambient temperature; regioselective oxidation

2: 90 percent / active zinc, pyridine / 0.03 h / Heating

With pyridine; ammonium cerium(IV) nitrate; zinc; In water; acetonitrile;