Technology Process of C40H32N2O4
There total 3 articles about C40H32N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydride; potassium iodide / dimethylformamide / 3 h / 70 °C
2: 850 mg / sodium hydroxide / ethanol; tetrahydrofuran; H2O / 4 h / 70 °C
3: thionyl chloride / benzene / 10 h / 60 °C
4: 182 mg / triethylamine / benzene / 4 h / 50 °C
With
sodium hydroxide; thionyl chloride; sodium hydride; triethylamine; potassium iodide;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo0340298
- Guidance literature:
-
Multi-step reaction with 2 steps
1: thionyl chloride / benzene / 10 h / 60 °C
2: 182 mg / triethylamine / benzene / 4 h / 50 °C
With
thionyl chloride; triethylamine;
In
benzene;
DOI:10.1021/jo0340298
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 850 mg / sodium hydroxide / ethanol; tetrahydrofuran; H2O / 4 h / 70 °C
2: thionyl chloride / benzene / 10 h / 60 °C
3: 182 mg / triethylamine / benzene / 4 h / 50 °C
With
sodium hydroxide; thionyl chloride; triethylamine;
In
tetrahydrofuran; ethanol; water; benzene;
DOI:10.1021/jo0340298