2,5-bis(chloromethyl)-3,4,6-trideuterionitrobenzene

Base Information

• Chemical Name: 2,5-bis(chloromethyl)-3,4,6-trideuterionitrobenzene
• CAS No.: 132734-00-0
• Molecular Formula: C₈H₇Cl₂NO₂
• Molecular Weight: 223.031
• Mol file: 132734-00-0.mol

Synonyms:

Chemical Property of 2,5-bis(chloromethyl)-3,4,6-trideuterionitrobenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,5-bis(chloromethyl)-3,4,6-trideuterionitrobenzene

There total 3 articles about 2,5-bis(chloromethyl)-3,4,6-trideuterionitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3,5,6-tetradeuterio-terephthalic acid dimethyl ester (74079-01-9) → 2,5-bis(chloromethyl)-3,4,6-trideuterionitrobenzene (132734-00-0)

Guidance literature:

Multi-step reaction with 3 steps

1: LiAlH₄ / tetrahydrofuran

2: 36 percent HCl

3: 60 percent HNO₃ / 96 percent H₂SO₄

With hydrogenchloride; lithium aluminium tetrahydride; sulfuric acid; nitric acid; In tetrahydrofuran;

Reference yield:

2,3,5,6-tetradeuteroterephthalic acid (60088-54-2) → 2,5-bis(chloromethyl)-3,4,6-trideuterionitrobenzene (132734-00-0)

Guidance literature:

Multi-step reaction with 4 steps

2: LiAlH₄ / tetrahydrofuran

3: 36 percent HCl

4: 60 percent HNO₃ / 96 percent H₂SO₄

With hydrogenchloride; lithium aluminium tetrahydride; sulfuric acid; nitric acid; In tetrahydrofuran;

Reference yield:

C8H6(2)H4O2 (1158734-28-1) → 2,5-bis(chloromethyl)-3,4,6-trideuterionitrobenzene (132734-00-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 36 percent HCl

2: 60 percent HNO₃ / 96 percent H₂SO₄

With hydrogenchloride; sulfuric acid; nitric acid;

upstream raw materials:

2,3,5,6-tetradeuterio-terephthalic acid dimethyl ester

2,3,5,6-tetradeuteroterephthalic acid

C₈H₆⁽²⁾H₄O₂