C₁₃H₁₄FN₃O₅S

Base Information

Chemical Name:C₁₃H₁₄FN₃O₅S
CAS No.:1353759-03-1
Molecular Formula:C₁₃H₁₄FN₃O₅S
Molecular Weight:343.336
Hs Code.:

C<sub>13</sub>H<sub>14</sub>FN<sub>3</sub>O<sub>5</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₄FN₃O₅S

Chemical Property:

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Technology Process of C₁₃H₁₄FN₃O₅S

There total 4 articles about C₁₃H₁₄FN₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353759-02-0
1,6-anhydro-3-azido-3-deoxy-4-O-tosyl-β-D-mannopyranose

: C₁₃H₁₄FN₃O₅S

: 1353759-03-1
C₁₃H₁₄FN₃O₅S

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane; at -50 - 20 ℃; optical yield given as %de;
DOI:10.1039/c1ob06336g

Reference yield:

: 213594-43-5
1,6:3,4-dianhydro-2-O-benzyl-β-D-altropyranose

: C₁₃H₁₄FN₃O₅S

: 1353759-03-1
C₁₃H₁₄FN₃O₅S

Guidance literature:: Multi-step reaction with 4 steps

1: lithium azide / N,N-dimethyl-formamide / 30 h / 110 °C / Inert atmosphere

2: pyridine / 48 h / 20 °C

3: potassium bromate; sodium dithionite / water; ethyl acetate / 5 h / 20 °C

4: diethylamino-sulfur trifluoride / dichloromethane / -50 - 20 °C

With pyridine; potassium bromate; sodium dithionite; lithium azide; diethylamino-sulfur trifluoride; In dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/c1ob06336g

Reference yield:

: 289505-45-9
1,6-Anhydro-3-azido-2-O-benzyl-3-deoxy-β-D-mannopyranose

: C₁₃H₁₄FN₃O₅S

: 1353759-03-1
C₁₃H₁₄FN₃O₅S

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 48 h / 20 °C

2: potassium bromate; sodium dithionite / water; ethyl acetate / 5 h / 20 °C

3: diethylamino-sulfur trifluoride / dichloromethane / -50 - 20 °C

With pyridine; potassium bromate; sodium dithionite; diethylamino-sulfur trifluoride; In dichloromethane; water; ethyl acetate;
DOI:10.1039/c1ob06336g