Technology Process of kyotorphin acetate salt
There total 7 articles about kyotorphin acetate salt which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 91 percent / Et3N / dimethylformamide / 48 h / 4 °C
2: 1) methane sulfonic acid, anisol,thioanisol, o-cresol / 1) RT, 60 min
With
methanesulfonic acid; methyl-phenyl-thioether; methoxybenzene; ortho-cresol; triethylamine;
In
N,N-dimethyl-formamide;
DOI:10.1248/cpb.28.1935
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 91 percent / Et3N / dimethylformamide / 48 h / 4 °C
2: 1) methane sulfonic acid, anisol,thioanisol, o-cresol / 1) RT, 60 min
With
methanesulfonic acid; methyl-phenyl-thioether; methoxybenzene; ortho-cresol; triethylamine;
In
N,N-dimethyl-formamide;
DOI:10.1248/cpb.28.1935
- Guidance literature:
-
Multi-step reaction with 3 steps
1: diazotizing reagent
2: 91 percent / Et3N / dimethylformamide / 48 h / 4 °C
3: 1) methane sulfonic acid, anisol,thioanisol, o-cresol / 1) RT, 60 min
With
methanesulfonic acid; methyl-phenyl-thioether; diazotizing reagent; methoxybenzene; ortho-cresol; triethylamine;
In
N,N-dimethyl-formamide;
DOI:10.1248/cpb.28.1935