Ru(NC₅H₄C₅H₄N)2(NC₅H₄NC₅H₃CCC₆H₂(OC₁₂H₂₅)2C₂C₆H₅)⁽²⁺⁾

Base Information

Chemical Name:Ru(NC₅H₄C₅H₄N)2(NC₅H₄NC₅H₃CCC₆H₂(OC₁₂H₂₅)2C₂C₆H₅)⁽²⁺⁾
CAS No.:870528-11-3
Molecular Formula:C₇₀H₈₀N₆O₂Ru
Molecular Weight:1138.51
Hs Code.:

Ru(NC<sub>5</sub>H<sub>4</sub>C<sub>5</sub>H<sub>4</sub>N)2(NC<sub>5</sub>H<sub>4</sub>NC<sub>5</sub>H<sub>3</sub>CCC<sub>6</sub>H<sub>2</sub>(OC<sub>12</sub>H<sub>25</sub>)2C<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)<sup>(2+)</sup>

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Chemical Property of Ru(NC₅H₄C₅H₄N)2(NC₅H₄NC₅H₃CCC₆H₂(OC₁₂H₂₅)2C₂C₆H₅)⁽²⁺⁾

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Technology Process of Ru(NC₅H₄C₅H₄N)2(NC₅H₄NC₅H₃CCC₆H₂(OC₁₂H₂₅)2C₂C₆H₅)⁽²⁺⁾

There total 1 articles about Ru(NC₅H₄C₅H₄N)2(NC₅H₄NC₅H₃CCC₆H₂(OC₁₂H₂₅)2C₂C₆H₅)⁽²⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 640727-04-4
Ru(NC₅H₄C₅H₄N)2(NC₅H₄NC₅H₃Br)⁽²⁺⁾

: 645414-32-0
2-[2',5'-bis(dodecyloxy)-4'-ethynylphenyl]ethynylbenzene

: 870528-11-3
Ru(NC₅H₄C₅H₄N)2(NC₅H₄NC₅H₃CCC₆H₂(OC₁₂H₂₅)2C₂C₆H₅)⁽²⁺⁾

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; under Ar; soln. of Ru complex and HCCC6H2(OC12H25)2C2C6H5 in DMF contg. Et3N introduced into sealed tube; degassed under Ar; Pd complex and CuI added; degassed; heated at 45°C for 18 h; H2O added; extd. with CH2Cl2; org. layer washed with H2O; dried (MgSO4);rotary evapd.; purified by flash chromy. (SiO2, CH2Cl2 to CH2Cl2-MeCN 8 0:20) and size exclusion chromy. (Sephadex LH-20, THF);
DOI:10.1039/b506837a